Preparation method of chitin composite bio-glass tissue repair material
A bioglass, tissue repair technology, applied in tissue regeneration, medical science, prosthesis, etc., can solve problems such as poor mechanical properties and poor drug adhesion, and achieve the effects of improving mechanical properties, good porosity, and improving medical properties.
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[0019] A preparation method of chitin composite biological glass tissue repair material, comprising the following steps:
[0020] Step 1: Weigh 10g of chitin and place it in a three-necked flask, and add 3mol / L hydrochloric acid solution, wherein the feeding ratio of chitin and hydrochloric acid solution is 1 / 30g·mL -1 , boil the mixed solution to reflux, stirring continuously during the process, after the reaction lasts for 6 hours, centrifuge the mixed solution and remove the upper liquid, take the lower precipitate and put it back into the three-necked flask and press 1 / 30g·mL -1 Add the feed ratio to 3mol / L hydrochloric acid solution, continue to heat and reflux for 6 hours, centrifuge the mixed solution and remove the upper liquid, take the lower sediment and wash it repeatedly with deionized water until the pH value reaches between 3-4. Add 100mL deionized water to the mixture for ultrasonic dispersion, then transfer the evenly dispersed dispersion to a dialysis bag with...
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