Protoporphyrin fluorescent carbon dot, and preparation method and application thereof
A fluorescent carbon dot, protoporphyrin technology, applied in the directions of botanical equipment and methods, applications, chemical instruments and methods, etc., to achieve the effects of good water solubility, low risk and mild reaction conditions
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Embodiment 1
[0026] The preparation method of protoporphyrin fluorescent carbon dots 1 comprises the following steps:
[0027] 1) Prepare 10 mL of PEI (Mn=550~650) solution of 2 mg / mL, weigh 10 mg of protoporphyrin, add them to the hydrothermal reactor together, and react at 220° C. for 10 h;
[0028] 2) After the reaction is completed, cool to room temperature, conduct dialysis with a 1000D dialysis bag for 3 days, and then filter the dialyzed product with a 0.22 μm pinhole filter, and the obtained filtrate is the protoporphyrin fluorescent carbon dots.
Embodiment 2
[0030] The preparation method of protoporphyrin fluorescent carbon dots 2 comprises the following steps:
[0031] 1) Prepare 10 mL of PEI (Mn=550~650) solution of 2 mg / mL, weigh 10 mg of protoporphyrin, add them to the hydrothermal reactor together, and react at 220° C. for 8 h;
[0032] 2) After the reaction is completed, cool to room temperature, conduct dialysis with a 1000D dialysis bag for 3 days, and then filter the dialyzed product with a 0.22 μm pinhole filter, and the obtained filtrate is the protoporphyrin fluorescent carbon dots.
Embodiment 3
[0034] The preparation method of protoporphyrin fluorescent carbon dots 3 comprises the following steps:
[0035] 1) Prepare 10 mL of PEI (Mn=550~650) solution of 2 mg / mL, weigh 10 mg of protoporphyrin, add them to the hydrothermal reactor together, and react at 180° C. for 8 h;
[0036] 2) After the reaction is completed, cool to room temperature, conduct dialysis with a 1000D dialysis bag for 3 days, and then filter the dialyzed product with a 0.22 μm pinhole filter, and the obtained filtrate is the protoporphyrin fluorescent carbon dots.
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