A kind of ultra-low density ceramsite proppant and preparation method thereof
An ultra-low density, proppant technology, applied in the gas well fracturing process proppant, oil field, can solve the problems of occupying land, environmental pollution, waste of resources, etc., to achieve large output, reduce production costs, reduce the use of Effect
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Embodiment 1
[0028] The ultra-low density ceramsite proppant described in this embodiment, the mass percent of raw material is as follows:
[0029] Calcined coal gangue 60%, uncalcined coal gangue 25%, alumina powder 11%, aluminum fluoride 1%, vanadium pentoxide 3%.
[0030] The raw material technical index is coal gangue (Al 2 o 3 :36.18wt%, SiO 2 :44.48 wt%, Fe 2 o 3 :0.34wt%, TiO 2 : 0.71wt%, CaO: 0.42wt%, K 2 O: 0.18wt%, Na 2 O: 0.034wt%, MgO: 0.19wt%, other burning loss); alumina powder (Al 2 o 3 content 90wt%); aluminum fluoride, vanadium pentoxide (content 99wt%).
[0031] The preparation steps are as follows:
[0032] The coal gangue is calcined at 600°C for 1.5 hours, and then crushed to obtain calcined gangue raw materials; it is weighed according to the mass percentage of the calcined coal gangue, uncalcined coal gangue, alumina powder, aluminum fluoride and vanadium pentoxide. After taking it, mix it evenly and grind it until the fineness is less than 400 meshes to o...
Embodiment 2
[0035] The ultra-low density ceramsite proppant described in this embodiment, the mass percent of raw material is as follows:
[0036] Calcined coal gangue 45%, uncalcined coal gangue 30%, alumina powder 20%, aluminum fluoride 3%, vanadium pentoxide 2%.
[0037] The raw material technical index is coal gangue (Al 2 o 3 :36.18wt%, SiO 2 :44.48 wt%, Fe 2 o 3 :0.34wt%, TiO 2 : 0.71wt%, CaO: 0.42wt%, K 2 O: 0.18wt%, Na 2 O: 0.034wt%, MgO: 0.19wt%, other burning loss); alumina powder (Al 2 o 3 content 80wt%); aluminum fluoride, vanadium pentoxide (content 99wt%).
[0038] The preparation steps are as follows:
[0039] The coal gangue is calcined at 750°C for 1 hour, and then crushed to obtain calcined gangue raw materials; weighed according to the mass percentage of the calcined coal gangue, uncalcined coal gangue, alumina powder, aluminum fluoride and vanadium pentoxide Afterwards, mix evenly and grind until the fineness is less than 400 meshes to obtain a mixed materia...
Embodiment 3
[0042] The ultra-low density ceramsite proppant described in this embodiment, the mass percent of raw material is as follows:
[0043] Calcined coal gangue 50%, uncalcined coal gangue 23%, alumina powder 20%, aluminum fluoride 2%, vanadium pentoxide 5%.
[0044] The raw material technical index is uncalcined coal gangue (Al 2 o 3 :36.18wt%, SiO 2:44.48 wt%, Fe 2 o 3 :0.34wt%, TiO 2 : 0.71wt%, CaO: 0.42wt%, K 2 O: 0.18wt%, Na 2 O: 0.034wt%, MgO: 0.19wt%, other burning loss); alumina powder (Al 2 o 3 content 80wt%); aluminum fluoride, vanadium pentoxide (content 99wt%).
[0045] The preparation steps are as follows:
[0046] The coal gangue is calcined at 900°C for 0.5h, and then crushed to obtain the calcined gangue raw material; it is weighed according to the mass percentage of the calcined coal gangue, uncalcined coal gangue, alumina powder, aluminum fluoride and vanadium pentoxide. After taking it, mix it evenly and grind it until the fineness is less than 400 mes...
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