Coal briquette adhesive employing defatted soybean protein as raw material and preparation method of coal briquette adhesive
A defatted soybean protein and adhesive technology, which is applied in the preparation of protein adhesives, animal glue or gelatin, adhesives, etc., can solve the problems of greatly reduced cold strength of briquettes, affecting the use of briquettes, and poor waterproof performance , to achieve the effect of low processing cost, convenient processing and good water resistance
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Embodiment 1
[0028] A briquette adhesive using defatted soybean protein as a raw material, the briquette adhesive is processed from the following raw materials in parts by weight:
[0029] 20 parts of cement, 80 parts of modified defatted soybean powder, 8 parts of organic bentonite, 8 parts of propolis powder, 400 parts of water;
[0030] The preparation method of the modified defatted soybean powder is as follows: add defatted soybean powder, an appropriate amount of complex enzyme and an appropriate amount of deionized water into the reaction vessel, adjust the pH to 5.5, enzymatically hydrolyze at 45°C for 2 hours, then heat to 85°C to inactivate 3min, cooled to 35°C, added 1% coupling agent and 0.5% oxidizing agent by mass of defatted soybean powder, stirred for 0.5h, filtered to remove impurities, concentrated in vacuum, and dried to obtain modified defatted soybean powder;
[0031] The compound enzyme is a mixture of cellulase, α-amylase and protease at an enzyme activity ratio of 5...
Embodiment 2
[0039] A briquette adhesive using defatted soybean protein as a raw material, the briquette adhesive is processed from the following raw materials in parts by weight:
[0040] 30 parts of cement, 120 parts of modified defatted soybean powder, 12 parts of organic bentonite, 12 parts of propolis powder, 600 parts of water;
[0041] The preparation method of the modified defatted soybean powder is as follows: add defatted soybean powder, an appropriate amount of complex enzyme and an appropriate amount of deionized water into the reaction vessel, adjust the pH to 6.0, enzymatically hydrolyze at 55°C for 2 hours, and then heat to 95°C to inactivate 2min, cooled to 35°C, added 2% coupling agent and 0.3% oxidizing agent by mass of defatted soybean powder, stirred for 1 hour, filtered to remove impurities, concentrated in vacuum, and dried to obtain modified defatted soybean powder;
[0042] The compound enzyme is a mixture of cellulase, α-amylase and protease at an enzyme activity r...
Embodiment 3
[0050] A briquette adhesive using defatted soybean protein as a raw material, the briquette adhesive is processed from the following raw materials in parts by weight:
[0051] 25 parts of cement, 100 parts of modified defatted soybean powder, 10 parts of organic bentonite, 10 parts of propolis powder, and 500 parts of water;
[0052]The preparation method of the modified defatted soybean powder is as follows: add defatted soybean powder, an appropriate amount of complex enzyme and an appropriate amount of deionized water into the reaction vessel, adjust the pH to 5.8, enzymatically hydrolyze at 50°C for 1.5h, then heat to 90°C to extinguish Live for 3 minutes, cool to 32°C, add 1.5% coupling agent and 0.4% oxidant by mass of defatted soybean powder, stir for 0.5h, filter to remove impurities, vacuum concentrate, and dry to obtain modified defatted soybean powder;
[0053] The compound enzyme is a mixture of cellulase, α-amylase and protease at an enzyme activity ratio of 5:1:1...
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