A kind of reactive dye fixing agent and preparation method thereof
A technology of reactive dyes and color-fixing agents, applied in dyeing, textile and papermaking, etc., can solve problems such as hue change, and achieve the effect of preventing falling off or hydrolysis, reducing water solubility, and no secondary pollution
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Embodiment 1
[0015] In the embodiment of the present invention, a reactive dye fixing agent is composed of the following raw materials in parts by weight: 41 parts of bisphenol S, 5 parts of dichloropropane, 10 parts of dimethylformamide, 17 parts of dimethyl sulfoxide, 3 parts of fatty alcohol polyoxyethylene ether, 13 parts of dichloroacetic acid.
[0016] Dichloroacetic acid and deionized water are mixed to prepare a dichloroacetic acid solution with a mass concentration of 17%; fatty alcohol polyoxyethylene ether is mixed with deionized water whose mass is 8.7 times to prepare a fatty alcohol polyoxyethylene ether solution. Mix bisphenol S with dimethyl sulfoxide and dimethyl formamide, heat up to 60°C, and stir at this temperature for 40 minutes, then add fatty alcohol polyoxyethylene ether solution, heat up to 94°C and Stir at low temperature for 22 minutes; then add dichloropropane, and stir at 65°C for 20 minutes; then add dichloroacetic acid solution dropwise in 5 minutes, and sti...
Embodiment 2
[0018] In the embodiment of the present invention, a reactive dye fixing agent is composed of the following raw materials in parts by weight: 49 parts of bisphenol S, 13 parts of dichloropropane, 18 parts of dimethylformamide, 25 parts of dimethyl sulfoxide, 7 parts of fatty alcohol polyoxyethylene ether, 21 parts of dichloroacetic acid.
[0019] Dichloroacetic acid and deionized water are mixed to prepare a dichloroacetic acid solution with a mass concentration of 17%; fatty alcohol polyoxyethylene ether is mixed with deionized water whose mass is 8.7 times to prepare a fatty alcohol polyoxyethylene ether solution. Mix bisphenol S with dimethyl sulfoxide and dimethyl formamide, heat up to 60°C, and stir at this temperature for 40 minutes, then add fatty alcohol polyoxyethylene ether solution, heat up to 94°C and Stir at low temperature for 22 minutes; then add dichloropropane, and stir at 65°C for 20 minutes; then add dichloroacetic acid solution dropwise in 5 minutes, and st...
Embodiment 3
[0021] In the embodiment of the present invention, a reactive dye fixing agent is composed of the following raw materials in parts by weight: 43 parts of bisphenol S, 7 parts of dichloropropane, 12 parts of dimethylformamide, 19 parts of dimethyl sulfoxide, 4 parts of fatty alcohol polyoxyethylene ether, 15 parts of dichloroacetic acid.
[0022] Dichloroacetic acid and deionized water are mixed to prepare a dichloroacetic acid solution with a mass concentration of 17%; fatty alcohol polyoxyethylene ether is mixed with deionized water whose mass is 8.7 times to prepare a fatty alcohol polyoxyethylene ether solution. Mix bisphenol S with dimethyl sulfoxide and dimethyl formamide, heat up to 60°C, and stir at this temperature for 40 minutes, then add fatty alcohol polyoxyethylene ether solution, heat up to 94°C and Stir at low temperature for 22min; then add dichloropropane, stir at 65°C for 20min; then add dichloroacetic acid solution dropwise in 5min, and stir at 78°C for 64min...
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