A kind of preparation method of multifunctional polyester fiber
A polyester fiber and multi-functional technology, which is applied in the field of preparation of multi-functional polyester fiber, can solve the problems of poor effect, high addition amount and difficult dispersion, etc., and achieve the effect of low cost, long-lasting effect and increased compatibility
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Embodiment 1
[0022] A kind of preparation method of multifunctional polyester fiber, concrete steps are:
[0023] The first step: Add 19.5g α-ZrP to 100 ml tetrahydrofuran, ultrasonically and mechanically stir, the ultrasonic power is 50W, the time is 20min; the speed of mechanical stirring is 200r / min, the time is 20min; 1.7g copper chloride is added In the solution, react for 6h; dropwise add the silane coupling agent KH550 to continue the reaction, the mass ratio of the amount of KH550 added to α-ZrP is 0.5:1; add nitric acid with a mass fraction of 80% to treat the multi-walled carbon nanotubes; the reaction temperature at 80°C, and the reaction time was 12 h. E51 was added to modify the acidified multi-walled carbon nanotubes; the molar ratio of acidified carbon material to epoxy modifier E51 was 1:5, the reaction temperature was 80 °C, and the reaction time was 12 h. The molar ratio of epoxy-modified multi-walled carbon nanotubes to KH550-α-ZrP is 1:1; the temperature is raised to 8...
Embodiment 2
[0026] A kind of preparation method of multifunctional polyester fiber, concrete steps are:
[0027] The first step: Add 19.5g α-ZrP to 100 ml DMF, ultrasonically and mechanically stir, the ultrasonic power is 35W, the time is 60 min; the speed of mechanical stirring is 300r / min, the time is 15min; 1.6g copper sulfate is added In the solution, react for 12 h; dropwise add silane coupling agent KH550 to continue the reaction, the mass ratio of the amount of KH550 added to α-ZrP is 1:1; add nitric acid with a mass fraction of 80% to treat the multi-walled carbon nanotubes; react The temperature was 75°C, and the reaction time was 24 h. E51 was added to modify the acidified multi-walled carbon nanotubes; the molar ratio of acidified carbon material to epoxy modifier E51 was 1:5, the reaction temperature was 75 °C, and the reaction time was 24 h. The molar ratio of epoxy-modified multi-walled carbon nanotubes to KH550-α-ZrP is 1:1; the temperature is raised to 80°C, and the react...
Embodiment 3
[0030] A kind of preparation method of multifunctional polyester fiber, concrete steps are:
[0031] Step 1: Add 19.5g α-ZrP to 100 ml tetrahydrofuran, ultrasonically and mechanically stir, the ultrasonic power is 50W, and the time is 30min; the speed of mechanical stirring is 300r / min, and the time is 30min; 0.85g silver nitrate is added to the solution During the reaction for 18 h; the silane coupling agent KH550 was added dropwise to continue the reaction, and the mass ratio of the amount of KH550 added to α-ZrP was 1:1; the mass fraction of 80% was added to treat nano-carbon black with nitric acid; the reaction temperature was 80 °C, and the reaction time was 12 h. E51 was added to modify acidified nano-carbon black; the molar ratio of acidified carbon material to epoxy modifier E51 was 1:5, the reaction temperature was 80 °C, and the reaction time was 24 h. The molar ratio of epoxy-modified multi-walled carbon nanotubes to KH550-α-ZrP is 1:1; the temperature is raised to...
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