Amphetamine tablet homogenization method

A homogenization technology of amphetamines, applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of reducing the accuracy and repeatability of drug detection, poor distribution uniformity of active ingredients, and poor production conditions, etc., to achieve crushing Good effect, good cleaning effect, reliable method

Inactive Publication Date: 2017-03-15
INST OF FORENSIC SCI OF MIN OF PUBLIC SECURITY
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  • Description
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  • Application Information

AI Technical Summary

Problems solved by technology

So far, my country has not formulated a corresponding homogenization standard method to standardize the sampling process. In practice, manual grinding with a mortar and bowl is the main method, which is highly random and poorly controllable, which reduces the accuracy and repeatability of drug testing.
Especially for amphetamine-type drug tablets, due to the poor production conditions and poor workmanship of underground processing plants, the distribution of active ingredients is very poor, and it is especially necessary to carry out artificial homogenization treatment to ensure the effectiveness of the sampling and testing pro...

Method used

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  • Amphetamine tablet homogenization method
  • Amphetamine tablet homogenization method
  • Amphetamine tablet homogenization method

Examples

Experimental program
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Embodiment Construction

[0046] The experimental methods used in the following examples are conventional methods unless otherwise specified.

[0047] The materials and reagents used in the following examples can be obtained from commercial sources unless otherwise specified.

[0048] The following examples take the methamphetamine tablet (the most common amphetamine tablet) as the experimental sample, and use the household mixer as the homogenization equipment of the tablet sample (simulated sample and actual sample), investigate the effect and The feasibility of the cleaning method, meanwhile, was compared with the traditional manual grinding method in a mortar and pestle. The relative standard deviation of the content of the target substance in the sample homogenized by a household mixer and the particle size of the pulverized sample are used as evaluation criteria to discuss the required mixing time; the evaluation standard is whether the target substance remains in the homogenization equipment , ...

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Abstract

The invention discloses an amphetamine tablet homogenization method which comprises the following steps: homogenization treatment is performed on an amphetamine tablet by utilizing a household stirrer; the household stirrer comprises a stirrer main body as well as a dry grinding cup and a dry grinding cutter base matched with the main body, and the dry grinding cutter base is matched with the main body of the stirrer; the amphetamine tablet is put into the dry grinding cup. The invention further provides a homogenization effect evaluation method. Quality control and evaluation are implemented from two aspects, that is, particle sizes of crushed sample granules, and relative standard deviation of contents of target substances in samples taken in different positions, thus being scientific and reasonable. The invention further establishes a method for washing the household stirrer for the amphetamine tablet, and provides parameters and a calculation method for evaluating a washing effect. Experiment shows that by adopting the methods, amphetamine drug tablet inspection requirements of international standard methods for quantitative and qualitative international standard methylamphetamine drug detection, industrial methods for MDMA (methylene dioxymetham-phetamine) drug detection can be met, a good washing effect can be achieved, and the methods are reliable.

Description

technical field [0001] The invention relates to a method for homogenizing amphetamine tablets. Background technique [0002] The qualitative and quantitative identification of drugs plays an important role in the investigation and litigation of drug cases, and is an important basis for the court to convict and sentence criminal suspects. The "Regulations on Several Issues Concerning the Examination and Judgment of Evidence in the Handling of Death Penalty Cases" and the "Regulations on Several Issues Concerning the Exclusion of Illegal Evidence in the Handling of Criminal Cases" were promulgated and implemented on July 1, 2010. Regulation. [0003] Seized drugs are the most critical physical evidence in drug cases, especially for cases with a large amount of drug trafficking and a large number of packages, how to carry out laboratory tests on seized drug samples in a representative, legal and standardized manner has become a concern in the investigation and litigation proce...

Claims

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Application Information

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IPC IPC(8): G01N30/02G01N30/06
CPCG01N30/02G01N30/06
Inventor 黄星翟晚枫王蔚昕常颖高利生
Owner INST OF FORENSIC SCI OF MIN OF PUBLIC SECURITY
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