Deinking agent
A technology of deinking agent and stripping agent, applied in the field of cleaning agents, can solve the problems of backward environmental testing and solutions, difficult cleaning of oil film, less research work, etc., achieve good deinking effect, good wettability, and reduce dosage Effect
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Embodiment 1
[0025] Embodiment 1: raw material preparation:
[0026] 1) The surfactant is obtained by esterification modification with succinic acid after amidation reaction of vegetable oil and organic base. Specifically, it is prepared by the following method: add the organic base into the reactor, add the catalyst and vegetable oil under stirring, control the mass ratio of the organic base, vegetable oil, and catalyst to 2.4:1:0.6, slowly raise the temperature to 120°C for 4 hours, and cool down to After room temperature, the amidation product was obtained; after that, the amidation product was added into the reactor, and succinic acid was added three times under stirring, and the molar ratio of carboxyl group to hydroxyl group was controlled to be 1:1.2. After feeding, the temperature was raised to 75°C for 4 hours. After cooling down to room temperature, a succinic modified product was obtained; 25 wt% aqueous ammonia solution was added dropwise to the succinic modified product, and s...
Embodiment 2
[0028] Embodiment 2: Raw material preparation: Surfactant is specifically prepared by the following method: add organic base in the reactor, add catalyst and vegetable oil under stirring, control the mass ratio of organic base, vegetable oil, catalyst to be 2.6:1:1, Slowly raise the temperature to 130°C and react for 3 hours. After cooling down to room temperature, the amidation product is obtained; then add the amidation product into the reactor, add succinic acid three times under stirring, control the molar ratio of carboxyl group to hydroxyl group to 1:1.4, and feed After the completion, the temperature was raised to 75°C for 4 hours, and after cooling down to room temperature, a succinic modified product was obtained; 28 wt% ammonia solution was added dropwise to the succinic modified product, and stirred for 45 minutes until the pH value was adjusted to 14 to obtain a surfactant B, where the organic base is a mixture of diethanolamine and ethyldiethanolamine at a ratio of...
Embodiment 3
[0029] Embodiment 3: Raw material preparation: Surfactant is specifically prepared by the following method: add organic base in the reactor, add catalyst and vegetable oil under stirring, control the mass ratio of organic base, vegetable oil, catalyst to be 2.5:1:0.8, Slowly raise the temperature to 110°C and react for 4 hours. After cooling down to room temperature, the amidation product is obtained; then add the amidation product into the reactor, add succinic acid three times under stirring, control the molar ratio of carboxyl group to hydroxyl group to 1:1.3, and feed After completion, the temperature was raised to 80°C for 3.5 hours, and after cooling down to room temperature, a succinic modified product was obtained; 30 wt% ammonia solution was added dropwise to the succinic modified product, and stirred for 55 minutes until the pH value was adjusted to 13 to obtain surface activity Agent C, wherein the organic base is triethanolamine; the catalyst is a mixture of tetraet...
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