Sewage purification device and purification method based on chemical neutralization method and nanofiltration technology
A nanofiltration and sewage purification technology, applied in chemical instruments and methods, neutralized water/sewage treatment, water/sewage treatment equipment, etc., can solve the problems of high treatment cost, long process flow, complicated control, etc., and achieve the purification effect Good, the effect of increasing the stirring uniformity rate and high integration
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Embodiment 1
[0048] According to the following steps to manufacture the stirring rotary teeth 1-11-5 of the present invention, and by weight fraction:
[0049] Step 1: Add 444 parts of ultrapure water with a conductivity of 0.44μS / cm into the reactor, start the stirrer in the reactor at a speed of 104rpm, start the heating pump, and raise the temperature in the reactor to 74°C; (E)-3-(3,4-dimethoxyphenyl)-2-ethyl cyanoacrylate 74 parts, 3,5-bis[(2,4-diaminophenyl)azo]-4 - 94 parts of sodium toluenesulfonate, 144 parts of 3-(4-hydroxy-3-methoxyphenyl) lanosterol-2-acrylate, stir until completely dissolved, adjust the pH value to 4.4, and turn the stirrer speed Adjust to 144rpm, the temperature is 104°C, and the esterification reaction takes 24 hours;
[0050] Step 2: Take 94 parts of 3,5-bis(1,1-dimethylethyl)-4-hydroxybenzoic acid-2,4-bis(1,1-dimethylpropyl)phenyl ester, L 84 parts of (-)-1-(4-methylthiophenyl)-2-amino-1,3-propanediol were pulverized, and the particle size of the powder ...
Embodiment 2
[0055] According to the following steps to manufacture the stirring rotary teeth 1-11-5 of the present invention, and by weight fraction:
[0056] Step 1: Add 1414 parts of ultrapure water with a conductivity of 0.84μS / cm into the reactor, start the stirrer in the reactor at a speed of 244rpm, start the heating pump, and raise the temperature in the reactor to 94°C; 144 parts of (E)-3-(3,4-dimethoxyphenyl)-2-ethyl cyanoacrylate, 3,5-bis[(2,4-diaminophenyl)azo]-4 - 144 parts of sodium toluenesulfonate, 344 parts of 3-(4-hydroxy-3-methoxyphenyl) lanosterol-2-acrylate, stir until completely dissolved, adjust the pH value to 8.4, and turn the stirrer speed Adjust to 244rpm, the temperature is 174°C, and the esterification reaction is 34 hours;
[0057] Step 2: Take 204 parts of 3,5-bis(1,1-dimethylethyl)-4-hydroxybenzoic acid-2,4-bis(1,1-dimethylpropyl)phenyl ester, L 144 parts of (-)-1-(4-methylthiophenyl)-2-amino-1,3-propanediol were pulverized, and the particle size of the po...
Embodiment 3
[0062] According to the following steps to manufacture the stirring rotary teeth 1-11-5 of the present invention, and by weight fraction:
[0063] Step 1: Add 914 parts of ultrapure water with a conductivity of 0.54μS / cm into the reactor, start the stirrer in the reactor at a speed of 154rpm, start the heating pump, and raise the temperature in the reactor to 84°C; 104 parts of (E)-3-(3,4-dimethoxyphenyl)-2-ethyl cyanoacrylate, 3,5-bis[(2,4-diaminophenyl)azo]-4 - 134 parts of sodium toluenesulfonate, 234 parts of 3-(4-hydroxy-3-methoxyphenyl) lanosterol-2-acrylate, stir until completely dissolved, adjust the pH value to 5.4, and turn the stirrer speed Adjust to 184rpm, the temperature is 134°C, and the esterification reaction is 32 hours;
[0064] Step 2: Take 154 parts of 3,5-bis(1,1-dimethylethyl)-4-hydroxybenzoic acid-2,4-bis(1,1-dimethylpropyl)phenyl ester, L 104 parts of (-)-1-(4-methylthiophenyl)-2-amino-1,3-propanediol were pulverized, and the particle size of the pow...
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