Visible light responding photocatalyst LiFe3Sn2O9 and preparation method thereof
A photocatalyst and visible light technology, applied in catalyst activation/preparation, chemical instruments and methods, chemical elements of heterogeneous catalysts, etc., can solve the problems of limited types of photocatalysts, low light conversion efficiency, difficult synthesis, etc., and achieve visible light response. The effect of wide frequency range, high light conversion efficiency and simple preparation method
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Embodiment 1
[0018] (1) Analyze pure chemical raw material Li 2 CO 3 , Fe 2 O 3 And SnO 2 The powder is LiFe 3 Sn 2 O 9 The composition of the weighing ingredients.
[0019] (2) Mix the raw materials prepared in step (1), put them into a ball mill tank, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind, take out and dry, and pass through a 200-mesh sieve.
[0020] (3) Pre-fire the uniformly mixed powder in step (2) at 1100°C, keep it for 6 hours, cool it naturally to room temperature, and then pulverize it with a ball mill to make the average particle diameter smaller than 2μm, to obtain LiFe 3 Sn 2 O 9 powder.
[0021] The prepared photocatalyst, under visible light with a wavelength greater than 420nm, the removal rate of methyl orange reached 96.8% in 60 minutes.
Embodiment 2
[0023] (1) Analyze pure chemical raw material Li 2 CO 3 , Fe 2 O 3 And SnO 2 The powder is LiFe 3 Sn 2 O 9 The composition of the weighing ingredients.
[0024] (2) Mix the raw materials prepared in step (1), put them into a ball mill tank, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind, take out and dry, and pass through a 200-mesh sieve.
[0025] (3) Pre-fire the uniformly mixed powder in step (2) at 1130°C, keep it for 6 hours, cool it naturally to room temperature, and then pulverize it by a ball mill to reduce the average particle diameter to less than 2μm, which is LiFe 3 Sn 2 O 9 powder.
[0026] The prepared photocatalyst has a removal rate of 98.6% for methyl orange in 60 minutes under the irradiation of visible light with a wavelength greater than 420nm.
Embodiment 3
[0028] (1) Analyze pure chemical raw material Li 2 CO 3 , Fe 2 O 3 And SnO 2 The powder is LiFe 3 Sn 2 O 9 The composition of the weighing ingredients.
[0029] (2) Mix the raw materials prepared in step (1), put them into a ball mill tank, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind, take out and dry, and pass through a 200-mesh sieve.
[0030] (3) Pre-fire the uniformly mixed powder in step (2) at 1150°C, keep it for 6 hours, cool it naturally to room temperature, and then pulverize it by a ball mill to reduce the average particle diameter to less than 2μm to obtain LiFe 3 Sn 2 O 9 powder.
[0031] The prepared photocatalyst has a removal rate of 97.5% for methyl orange under the irradiation of visible light with a wavelength greater than 420nm in 60 minutes.
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