Hydrophobic pesticide preparation containing microcapsules and preparation method of hydrophobic pesticide preparation containing microcapsules
A pesticide preparation and microcapsule technology, which is applied in the field of hydrophobic pesticide preparations containing microcapsules and its preparation, can solve the problems of low utilization rate of emulsifiable concentrate formulations and serious environmental pollution, and achieve reduced spraying times, less investment in equipment, and easy operation. simple effect
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Embodiment 1
[0021] Accurately weigh 0.5g of polylactic acid-glycolic acid copolymer and 0.5g of acetochlor technical solution in 9g of acetone, that is, organic phase A; prepare 50mL, 1wt% sodium dodecylbenzenesulfonate solution as aqueous phase B ; Use a syringe to slowly drop into the water phase B at a rate of 5 drops per second. During the dropping process, keep the temperature at 25°C and stir at a rate of 700rpm; A mixed preparation of microcapsule suspension and acetochlor aqueous emulsion. The drug encapsulation rate of the mixed preparation was 19.2%, and the drug loading was 12.3% by mass.
Embodiment 2
[0023] Accurately weigh 0.4g of polylactic acid-glycolic acid copolymer and 0.6g of acetochlor technical solution in 9g of acetone, that is, organic phase A; prepare 50mL, 1wt% sodium dodecylbenzenesulfonate solution as aqueous phase B ; Use a syringe to slowly drop into the water phase B at a rate of 5 drops per second. During the dropping process, keep the temperature at 25°C and stir at a rate of 700rpm; A mixed preparation of microcapsule suspension and acetochlor aqueous emulsion. The drug encapsulation rate of the mixed preparation was 27.3%, and the drug loading was 16.8% by mass.
Embodiment 3
[0025] Accurately weigh 0.5g of polycaprolactone and 0.5g of chlorpyrifos technical substance and dissolve in 9g of acetone, that is, organic phase A; prepare 50mL, 1wt% sodium dodecylbenzenesulfonate solution as aqueous phase B; Add slowly at a rate of 5 drops per second to the aqueous phase B. During the dropping process, keep the temperature at 25°C and stir at a rate of 700rpm; Mixed formulation of chlorpyrifos emulsion in water. The drug encapsulation rate of the mixed preparation is 22.4%, and the drug loading is 13.5% by mass.
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