Preparation method and product of an organometallic complex and an alumina complex
A technology of organometallic and inorganic oxides, which is applied in the field of preparation of organometallic complexes and alumina complexes, can solve problems such as low surface active points, battery structure damage, failure, etc., achieve improved atomic structure composition, and simple preparation methods Practical, outstanding effect of water absorption
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Embodiment 1
[0035] An organometallic complex consisting of bis(2-methyl-8-hydroxyquinoline-N1,O8)-(1,1'-biphenyl-4-hydroxyl)aluminum (CAS146162-54-1, molecular formula C 32 h 25 AlN 2 o 3 ) and 8-hydroxyquinoline aluminum (C 27 h 18 AlN 3 o 3 ) composition, the mixing weight ratio of the two (2-methyl-8-hydroxyquinoline-N1, O8)-(1,1'-biphenyl-4-hydroxyl) aluminum and 8-hydroxyquinoline aluminum is 2:8.
[0036] The preparation method of above-mentioned organometallic complex, concrete steps are as follows:
[0037] (1) Weigh bis(2-methyl-8-hydroxyquinoline-N1,O8)-(1,1'-biphenyl-4-hydroxy)aluminum and 8-hydroxyquinoline aluminum as raw materials according to the recipe ;
[0038] (2) Mix the weighed bis(2-methyl-8-hydroxyquinoline-N1,O8)-(1,1'-biphenyl-4-hydroxy)aluminum with 8-hydroxyquinoline aluminum, Instantly.
Embodiment 2
[0040] An organometallic complex consisting of bis(2-methyl-8-hydroxyquinoline-N1,O8)-(1,1'-biphenyl-4-hydroxyl)aluminum (CAS146162-54-1, molecular formula C 32 h 25 AlN 2 o 3 ) and 8-hydroxyquinoline aluminum (C 27 h 18 AlN 3 o 3 ) composition, the mixing weight ratio of the two (2-methyl-8-hydroxyquinoline-N1, O8)-(1,1'-biphenyl-4-hydroxyl) aluminum and 8-hydroxyquinoline aluminum is 5:5.
[0041] The preparation method of above-mentioned organometallic complex, concrete steps are as follows:
[0042](1) Weigh bis(2-methyl-8-hydroxyquinoline-N1,O8)-(1,1'-biphenyl-4-hydroxy)aluminum and 8-hydroxyquinoline aluminum as raw materials according to the recipe ;
[0043] (2) Mix the weighed bis(2-methyl-8-hydroxyquinoline-N1,O8)-(1,1'-biphenyl-4-hydroxy)aluminum with 8-hydroxyquinoline aluminum, Instantly.
Embodiment 3
[0045] An organometallic complex consisting of bis(2-methyl-8-hydroxyquinoline-N1,O8)-(1,1'-biphenyl-4-hydroxyl)aluminum (CAS146162-54-1, molecular formula C 32 h 25 AlN 2 o 3 ) and 8-hydroxyquinoline aluminum (C 27 h 18 AlN 3 o 3 ) composition, the mixing weight ratio of the two (2-methyl-8-hydroxyquinoline-N1, O8)-(1,1'-biphenyl-4-hydroxyl) aluminum and 8-hydroxyquinoline aluminum is 2:5.
[0046] The preparation method of above-mentioned organometallic complex, concrete steps are as follows:
[0047] (1) Weigh bis(2-methyl-8-hydroxyquinoline-N1,O8)-(1,1'-biphenyl-4-hydroxy)aluminum and 8-hydroxyquinoline aluminum as raw materials according to the recipe ;
[0048] (2) Mix the weighed bis(2-methyl-8-hydroxyquinoline-N1,O8)-(1,1'-biphenyl-4-hydroxy)aluminum with 8-hydroxyquinoline aluminum, Instantly.
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