Method for making open-cell paraffin for polyurethane foam caulk
A technology of polyurethane foam and production method, which is applied in the direction of petrochemical modification, etc., can solve the problems of increased closed-cell ratio, decreased air permeability, and accelerated full drying speed of polyurethane foam, so as to reduce product quality problems and increase open cell ratio. , the effect of increasing air permeability
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Embodiment 1
[0020] A method for making open-cell paraffin for polyurethane foam caulking agent, adding heavy liquid wax into the reaction kettle, then feeding chlorine gas into the reaction kettle, controlling the flow rate of chlorine gas at 28m 3 / h, because the heat is released when the heavy liquid wax reacts with chlorine, as the reaction proceeds, the temperature in the reactor will increase. When the temperature in the reactor rises to 50°C, it will rise to this The temperature takes about 1.5 hours, and then use cooling water to control the reactor, so that the temperature in the reactor slowly rises to 55 ° C, and react at this temperature for 5.5 hours, during this period, the flow of chlorine gas is still controlled at 28cm 3 / h.
[0021] When the temperature in the reactor is 55°C, after reacting for 5.5 hours, increase the flow rate of chlorine gas to make the flow rate of chlorine gas reach 38m 3 / h, raise the temperature in the reactor to 65°C, and react at this temperatur...
Embodiment 2
[0028] A method for making open-cell paraffin for polyurethane foam caulking agent, adding heavy liquid wax into the reaction kettle, then feeding chlorine gas into the reaction kettle, controlling the flow rate of chlorine gas at 30m 3 / h, because the heat is released when the heavy liquid wax reacts with chlorine, as the reaction proceeds, the temperature in the reactor will increase. When the temperature in the reactor rises to 52°C, it will rise to this The temperature takes about 2 hours, and then the cooling water is used to control the reactor, so that the temperature in the reactor is slowly raised to 60°C, and the reaction is carried out at this temperature for 6 hours. During this time period, the flow rate of chlorine gas is still controlled at 30cm 3 / h.
[0029] When the temperature in the reactor is 60°C, after reacting for 6 hours, increase the flow rate of chlorine gas to make the flow rate of chlorine gas reach 40m 3 / h, the temperature in the reactor is rais...
Embodiment 3
[0036] A method for making open-cell paraffin for polyurethane foam caulking agent, adding heavy liquid wax into the reaction kettle, then feeding chlorine gas into the reaction kettle, controlling the flow rate of chlorine gas at 32m 3 / h, because the heat is released when the heavy liquid wax reacts with chlorine, as the reaction proceeds, the temperature in the reactor will increase. When the temperature in the reactor rises to 55°C, it will rise to this The temperature takes about 2.5 hours, and then use cooling water to control the reactor, so that the temperature in the reactor slowly rises to 65 ° C, and react at this temperature for 6.5 hours. During this period, the flow of chlorine gas is still controlled at 32cm 3 / h.
[0037] When the temperature in the reactor is 65°C, after reacting for 6.5 hours, increase the flow rate of chlorine gas to make the flow rate of chlorine gas reach 42m 3 / h, raise the temperature in the reactor to 75°C, and react at this temperatur...
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