Preparation process of modified paraffin for hardwood table and chair coating materials
A preparation process and modification technology, which is applied in the field of modified paraffin wax preparation process, can solve the problems of weakening the decorative effect of paraffin wax-based coatings, labor and labor, etc., and achieve the advantages of improving easy migration, improving heat resistance, and increasing endothermic peak temperature Effect
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Embodiment 1
[0020] A modified paraffin wax preparation process for hardwood table and chair coatings, comprising the following steps:
[0021] S1: Chop 50g of refined paraffin into small pieces and put them into a four-neck flask, heat, melt, stir and keep warm in a water bath at 75-85°C;
[0022] S2: Take 8-12 g of methyl acrylate monomer and add it dropwise into a four-necked flask, while feeding high-purity N 2 Protection, the methyl acrylate monomer has dissolved 0.5~0.7g initiator; In the present embodiment, the initiator adopts AIBN;
[0023] S3: heat preservation and reaction for a period of time, pour out the reactant in the flask while hot, and obtain the crude product of graft copolymer;
[0024] S4: Precipitate and separate the product with acetone, wash for several times, and dry to constant mass to obtain the grafted paraffin essence product, namely modified paraffin.
Embodiment 2
[0026] A modified paraffin wax preparation process for hardwood table and chair coatings, comprising the following steps:
[0027] S1: Chop 50g of refined paraffin into cube-shaped pieces with a side length of 0.5cm and put them into a four-neck flask, heat, melt, stir and keep warm in a water bath at 75-85°C;
[0028] S2: Take 10g of methyl acrylate monomer and add it dropwise into a four-necked flask, while feeding high-purity N 2 protection, the methyl acrylate monomer has dissolved 0.6g initiator; in the present embodiment, the initiator adopts AIBN, and when selecting AIBN as the initiator, the initiation efficiency of AIBN is higher, thereby the modified paraffin product has higher grafting rate, and the softening temperature is higher;
[0029] S3: Insulate and react for 5-8 minutes, pour out the reactant in the flask while it is hot, and obtain the crude graft copolymer product;
[0030] S4: Precipitate and separate the product with acetone, wash for several times, a...
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