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New bast fiber pectin degumming processing method

A processing method and hemp fiber technology, applied in the field of new hemp fiber pectin degumming processing, can solve the problems of affecting cellulose quality, long processing time, and affecting processing efficiency, so as to improve production efficiency, shorten processing technology, and achieve high efficiency. The effect of damage to degummed fibers

Inactive Publication Date: 2016-04-20
宿州学院
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Different hemp contains different colloids, so the processing methods required are also different. Although the current chemical methods used to remove pectin can remove pectin, they do great damage to cellulose, and the processing time is very long , which greatly affects the processing efficiency and the quality of the processed cellulose

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Embodiment 1: the present embodiment carries out as follows:

[0020] Step 1: acid leaching: put the raw hemp into water, then add dilute sulfuric acid, the concentration of sulfuric acid after adding is 0.5ml / L, then heat to 35°C for 50min;

[0021] Step 2: Washing: Take out the raw hemp after acid leaching and rinse it twice with water, 10 minutes each time;

[0022] Step 3: Pre-degumming:

[0023] 1. Put water in the steamer and heat the water to 90°C, then put in the pre-washed raw hemp, then continue to heat the water, add the pre-degumming potion when it reaches 150°C, the pre-degumming potion contains Sodium thiosulfate, sulfuric acid, potassium chloride, the ratio between them is 6:1:0.6 respectively, and the concentration after adding the pre-degumming syrup is 0.3ml / L, then continue to heat the water for 60 minutes and keep it at 150°C, Finally, let it cool naturally to 95°C;

[0024] 2. Then heat the water up to 135°C for the second time, and then cool dow...

Embodiment 2

[0032] Embodiment 2: the present embodiment carries out as follows:

[0033] Step 1: Acid leaching: Put the raw hemp into water, then add dilute sulfuric acid, the concentration of sulfuric acid after adding is 1.0ml / L, then heat to 45°C for 40 minutes;

[0034] Step 2: Washing: Take out the raw hemp after acid leaching and rinse it twice with water, 10 minutes each time;

[0035] Step 3: Pre-degumming:

[0036] 1. Put water in the steamer and heat the water to 80°C, then put in the pre-washed raw hemp, then continue to heat the water, add the pre-degumming potion when it reaches 150°C, the pre-degumming potion contains Sodium thiosulfate, sulfuric acid, potassium chloride, the ratio between them is 6:1:0.6 respectively, and the concentration after adding the pre-degumming syrup is 0.5ml / L, then continue to heat the water for 60 minutes and keep it at 150°C, Finally, let it cool naturally to 95°C;

[0037] 2. Then heat the water up to 135°C for the second time, and then coo...

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PUM

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Abstract

The invention discloses a new bast fiber pectin degumming processing method. The new bast fiber pectin degumming processing method comprises the following steps: placing original hemp in water, adding dilute sulphuric acid, heating to 35 to 45 DEG C and soaking for 40 to 50 minutes; taking out the original hemp which is soaked with acid and rinsing twice; heating water to 80 to 90 DEG C in a steamer, placing the original hemp in the water, adding a pre-degumming solution at 150 DEG C, continuing heating for 60 minutes, and cooling to 95 DEG C; heating to 135 DEG C and steaming for 10 minutes; heating to 110 DEG C and steaming for 25 minutes; rinsing the pre-degummed original hemp twice; heating water to 70 to 80 DEG C in the other steamer, placing the pre-degummed original hemp in the steamer, adding a degumming solution at 120 DEG C, heating the water for 50 minutes, and finally cooling to 90 DEG C; heating to 115 DEG C and steaming for 10 minutes; heating to 110 DEG C and steaming for 20 minutes; and cooling to room temperature and rinsing the original hemp three times. According to the method disclosed by the invention, the processed fibers are complete; pectin is removed completely; the damage to the fibers is low; the process time is greatly shortened; and the production efficiency is remarkably improved.

Description

Technical field: [0001] The invention relates to the technical field of hemp fiber production, in particular to a new pectin degumming processing method for hemp fiber. Background technique: [0002] Hemp crops can be used as raw materials for chemical industry, medicine and papermaking. All hemp fibers are cellulose fibers, the basic chemical composition is cellulose, and other non-fibers such as pectin, hemicellulose, lignin, and fat wax Substances, these are collectively referred to as "colloid", hemp fibers are bonded into sheets by colloid, and they are all associated with cellulose. To take out available fibers, the colloid must be removed to separate the fibers, so it is called is called degumming. Different hemp contains different colloids, so the processing methods required are also different. Although the current chemical methods used to remove pectin can remove pectin, they do great damage to cellulose, and the processing time is very long , thus greatly affecti...

Claims

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Application Information

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IPC IPC(8): D01C1/02
CPCD01C1/02
Inventor 邓福康
Owner 宿州学院
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