Emulsified waste water treatment oil removing agent and preparation method and use method thereof

A technology for emulsifying wastewater and clearing oil, applied in separation methods, grease/oily substances/suspton removal devices, liquid separation, etc., can solve the problem of poor treatment effect of high-temperature emulsified sewage, affecting normal production process, clogging of air flotation aerators, etc. problem, to achieve significant treatment effect, good stability of treatment effect, and small dosage

Inactive Publication Date: 2016-04-20
LANZHOU YISHUN CHEM PROD CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the commonly used treatment methods for emulsified wastewater with better treatment effects include chemical dosing and process treatment. The chemical used in the dosing treatment is not effective in treating the emulsion at high temperature, and the process treatment basically uses two methods: grille and air flotation. This method is not effective for high-temperature emulsified sewage treatment, and when the oil content is high, the air flotation aerator head will be blocked and the normal production process will be affected.

Method used

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  • Emulsified waste water treatment oil removing agent and preparation method and use method thereof
  • Emulsified waste water treatment oil removing agent and preparation method and use method thereof
  • Emulsified waste water treatment oil removing agent and preparation method and use method thereof

Examples

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Effect test

preparation Embodiment 4

[0018] Example 4 of preparation of oil clearing agent for emulsified wastewater treatment: According to the data in Table 1, formula 4, 95.95 grams of water was poured into the reactor, and 0.03 grams of glycerin was added while stirring in the water, and the stirring was continued for at least 10 minutes; Add 0.95 grams of sodium silicate to the solution while stirring, and continue to stir for at least 20 minutes; add 0.07 grams of polydiallyldimethylammonium chloride to the solution obtained in the above steps, heat to 30 ° C and stir for 3 hours; Add 1.40 gram of magnesium sulfate, 1.60 gram of aluminum potassium sulfate successively while stirring in the solution that above-mentioned steps obtains, after continuing to stir for 2 hours, cool to room temperature to obtain emulsified waste water treatment clear oil agent, this emulsified waste water treatment oil clear agent is light yellow liquid visually, pH Value 7.2.

preparation Embodiment 5

[0019] Example 5 of preparation of oil clearing agent for emulsified wastewater treatment: According to the data in Table 1, formula 5, 95.95 grams of water was poured into the reactor, and 0.04 grams of glycerol was added while stirring in the water, and the stirring was continued for at least 10 minutes; Add 0.95 grams of sodium silicate to the solution while stirring, and continue to stir for at least 20 minutes; add 0.06 grams of polydiallyldimethylammonium chloride to the solution obtained in the above steps, heat to 30 ° C and stir for 3 hours; Add 1.20 grams of magnesium sulfate and 1.80 grams of potassium aluminum sulfate successively to the solution obtained in the above steps while stirring, and then continue to stir for 2 hours and then cool to room temperature to obtain an emulsified wastewater treatment oil clearing agent. Value 7.2.

preparation Embodiment 6

[0020] Example 6 of preparation of oil clearing agent for emulsified wastewater treatment: According to the data in Table 1, formula 6, 95.89 grams of water was poured into the reaction kettle, and 0.05 grams of glycerin was added while stirring in the water, and the stirring was continued for at least 10 minutes; to the above steps to obtain Add 1.00 g of sodium silicate to the solution while stirring, and continue to stir for at least 20 minutes; add 0.06 g of polydiallyldimethylammonium chloride to the solution obtained in the above steps, heat to 30 ° C and stir for 3 hours; Add 1.00 gram of magnesium sulfate and 2.00 gram of potassium aluminum sulfate successively to the solution obtained in the above steps while stirring, and then continue to stir for 2 hours and then cool to room temperature to obtain an emulsified wastewater treatment oil clearing agent, which is a colorless liquid by visual inspection, pH Value 7.3.

[0021] When the emulsified waste water treatment o...

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Abstract

The invention discloses an emulsified waste water treatment oil removing agent and a preparation method and use method thereof. The emulsified waste water treatment oil removing agent is prepared from, by weight, 0.02% to 0.05% of glycerol, 0.06% to 0.08% of poly(diallyldimethylammonium chloride), 0.80% to 1.00% of sodium silicate, 1.00% to 2.00% of magnesium sulfate, 1.00% to 2.00% of aluminum potassium sulfate and 95.89% to 96.10% of water. The content of oil, suspended solids, COD and other pollutants in emulsified waste water treated through the emulsified waste water treatment oil removing agent is greatly reduced, and when the emulsified waste water treatment oil removing agent is used, the feeding quantity is small, and treatment cost is low. Waste oil can be recycled after being treated, the waste water reaches the standard, and benefits can also be created. When the emulsified waste water treatment oil removing agent is applied, equipment modification is very small, investment is small, and the treatment effect is remarkable. The treatment operation is easy, high reliability is achieved, and management is facilitated. The emulsified waste water treatment oil removing agent is free of toxins, harm and secondary pollution, and up-to-standard emissions of the waste water can be ensured. The treatment effect is good in stability, and popularization is facilitated. The application range is wide, the recovery rate of oil products can be increased, the oil content in drained water can be reduced, and stable running of subsequent treatment units is promoted.

Description

technical field [0001] The invention relates to an industrial emulsified wastewater treatment agent, in particular to an emulsified wastewater treatment deoiling agent and a preparation method and application method thereof. Background technique [0002] Some production units of refining and chemical enterprises will produce a large amount of high-temperature oil-containing emulsified sewage during the production process. The instability of the sewage will lead to serious emulsification of sewage and increase the difficulty of treatment. If the sewage is directly discharged, it will cause great pollution to the environment, and if it enters the sewage treatment plant, it will also have a relatively large impact on the sewage treatment plant. Therefore, it needs to be pretreated and then sent to the sewage treatment plant for advanced treatment, and discharged after reaching the standard. [0003] At present, the commonly used treatment methods for emulsified wastewater with...

Claims

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Application Information

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IPC IPC(8): C02F1/40
CPCC02F1/40
Inventor 王倩
Owner LANZHOU YISHUN CHEM PROD CO LTD
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