Method for extracting cordyceps sinensis extract
A technology of Cordyceps sinensis and an extraction method is applied in the directions of pharmaceutical formulations, plant raw materials, medical preparations containing active ingredients, etc., and can solve the problems of increased extraction cost and low extraction rate.
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Embodiment 1
[0019] A method for extracting Cordyceps sinensis extract, comprising the following steps:
[0020] S1, washing Cordyceps sinensis, removing impurities, drying in the air, then drying at 30°C, crushing to 20-35 meshes to obtain Cordyceps sinensis micropowder;
[0021] S2. Add Cordyceps micropowder into the hydrochloric acid solution with a pH value of 5, heat up to 35°C and sonicate for 3 minutes, adjust the pH of the system to 7 and then sonicate for 10 minutes, adjust the pH of the system to 8 and then sonicate for 10 minutes, and heat up to 60°C , adding ethanol so that the volume of ethanol is 45% of the total volume of the system, ultrasonication for 10 min, then microwave at 50°C for 50 s, and filter to obtain the extract;
[0022] S3. Concentrating the extract under reduced pressure to a solid content of 85% to obtain the Cordyceps sinensis extract.
Embodiment 2
[0024] A method for extracting Cordyceps sinensis extract, comprising the following steps:
[0025] S1, washing Cordyceps sinensis, removing impurities, drying in the air, then drying at 35°C, crushing to 20-35 meshes to obtain Cordyceps sinensis micropowder;
[0026] S2. Add the micropowder of Cordyceps sinensis into the nitric acid solution with a pH value of 3, heat up to 38°C and sonicate for 8 minutes, adjust the pH of the system to 7 and then sonicate for 6 minutes, adjust the pH of the system to 10 and then sonicate for 7 minutes, heat up to 67°C , adding ethanol so that the volume of ethanol is 38% of the total volume of the system, ultrasonication for 22min, then microwave at 46°C for 66s, and filter to obtain the extract;
[0027] S3. Concentrating the extract under reduced pressure to a solid content of 89% to obtain the Cordyceps sinensis extract.
Embodiment 3
[0029] A method for extracting Cordyceps sinensis extract, comprising the following steps:
[0030] S1, washing Cordyceps sinensis, removing impurities, drying in the air, then drying at 42°C, crushing to 20-35 meshes to obtain Cordyceps sinensis micropowder;
[0031] S2. Add the micropowder of Cordyceps sinensis into the mixture of phosphoric acid solution and oxalic acid solution with a pH value of 4, heat up to 42°C and sonicate for 5 minutes, adjust the pH of the system to 7 and then sonicate for 8 minutes, and use triethylamine to adjust the pH of the system. After 9, sonicate for 8 minutes, heat up to 63°C, add ethanol so that the volume of ethanol is 42% of the total volume of the system, sonicate for 16 minutes, then microwave at 48°C for 58s, and obtain the extract after filtration; wherein, in the process of ultrasonic , the ultrasonic power is 900W;
[0032] S3. Concentrating the extract under reduced pressure to a solid content of 92% to obtain the Cordyceps sinen...
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