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Rapid catalysis dyeing paper manufacturing method

A manufacturing method, a technology of dyed paper, applied in papermaking, textiles and papermaking, adding inorganic compounds, etc., can solve the problems of inconspicuous soaking effect, non-compliance with continuous production of enterprises, and dim color of dyed paper, so as to increase market competition Power, improve the utilization rate of dye, the effect of golden and bright color

Active Publication Date: 2015-12-23
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Dyeing paper has developed rapidly in China in recent years, and the domestic demand is relatively large, but the production cost of the product is too high, the color of the product is not bright enough, the combination of dye and fiber is not sufficient, resulting in a large amount of waste of dye, hindering the health of the dyed paper industry develop
At present, the production of dyed paper mainly adopts the method of adding dyes to achieve the required bright color, but due to the existence of lignin, the color of the product will be dark. At the same time, we know that the coloring principle of dyes is the principle of subtractive color method. The more dyes are added More, the less bright the color will be, and adding too much dye will increase the production cost
[0003] There are also some enterprises that can achieve results through long-term reduction soaking, but the effect of long-term soaking is still not obvious, and it does not meet the requirements of continuous production of enterprises
[0004] The color of existing dyed paper is generally dull, the production cost is high, the amount of dyestuff is large and the utilization is insufficient, causing serious water pollution. This new technology meets the technical requirements of industrial production, the process is simple, and the cost is low. At present, there is no such kind at home and abroad. report on manufacturing method

Method used

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Examples

Experimental program
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Effect test

Embodiment 1

[0028] A kind of manufacture method of rapid catalytic dyeing paper, comprises following steps and technological condition:

[0029] (1) Stirring of slurry: directly pass the bamboo pulp after beating into the slurry tank, and rotate and stir at a speed of 30 revolutions per minute, so that 25°C is maintained in the slurry tank to provide the required chemicals for the next step of adding chemicals. Reaction temperature, after adding, stir slowly for 1 minute to fully react the solution and slurry;

[0030] (2) Oxidation of slurry: oxidant is dissolved, configuration mass fraction is the aqueous solution of 3%, oxidant is percarbamide, adds 5 liters of this oxidant aqueous solution in every ton of bamboo pulp (absolute dry pulp), slowly stirs 1 minute after adding , to fully react the solution and slurry.

[0031] (3) Acidification of the slurry: After the slurry reacts with the oxidant, the fibers need to be reduced again. The reducing drugs used are preferably used in acidi...

Embodiment 2

[0038]A kind of manufacture method of fast catalytic dyeing paper is characterized in that comprising following steps and process condition:

[0039] (1) Stirring of the slurry: directly pass the beaten bamboo pulp into the pulp pool, and rotate and stir at a speed of 30 revolutions per minute to keep 35°C in the pulp pool; provide the required chemical for the next step. Reaction temperature, after adding, stir slowly for 2 minutes to fully react the solution and the slurry;

[0040] (2) Oxidation of the slurry: dissolving the oxidizing agent, configuring a mass fraction of 4% aqueous solution, the oxidizing agent is thiourea dioxide; adding 6 liters of an oxidizing agent aqueous solution in every ton of absolute dry pulp, and slowly stirring for 5 minutes after adding to make the solution Fully react with the slurry;

[0041] (3) Acidification of the slurry: add 10 liters of citric acid solution with a concentration of 80%, and control the pH value to 5; stir slowly after a...

Embodiment 3

[0044] A kind of manufacture method of fast catalytic dyeing paper is characterized in that comprising following steps and process condition:

[0045] (1) Stirring of the slurry: directly pass the beaten bamboo pulp into the pulp pool, and rotate and stir at a speed of 40 revolutions per minute to keep 30°C in the pulp pool; to provide the required chemical for the next step. Reaction temperature, after adding, stir slowly for 5 minutes to fully react the solution and slurry;

[0046] (2) Oxidation of the slurry: dissolving the oxidizing agent, configuring an aqueous solution with a mass fraction of 5%, and the described oxidizing agent is percarbamide; 8 liters of an oxidizing agent aqueous solution are added in every ton of absolute dry pulp, and slowly stirred for 5 minutes after adding, so that The solution and the slurry fully react;

[0047] (3) Acidification of the slurry: add 7 liters of hydrochloric acid solution with a concentration of 80%, and control the pH value ...

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Abstract

The present invention discloses a rapid catalysis dyeing paper manufacturing method, which comprises: (1) slurry stirring: directly introducing a bamboo slurry being subjected to slurry beating into a slurry pool, stirring, and controlling the temperature of the slurry in the slurry pool at 20-50 DEG C; (2) slurry oxidation: dissolving an oxidant, preparing an aqueous solution, and carrying out a stirring reaction; (3) slurry acidification: adding hydrochloric acid, nitric acid or a citric acid solution, controlling the pH value of the slurry, and stirring to make the solution and the slurry be subjected to a complete reaction; and (4) slurry reduction: adding a reducing agent aqueous solution, carrying out a stirring reaction, adding auramine O to adjust the color when the slurry achieves a bright yellow color, preparing the pulp, carrying out papermaking, drying, cutting, and packaging. According to the present invention, through the oxidation reduction catalysis system, the color of the bamboo slurry can be changed into the golden yellow color within five minutes, the dye consumption during the yellow paper production process can be substantially reduced, the attach rate of the dye on the fibers can be improved, and the paper color can be bright.

Description

technical field [0001] The present invention relates to a manufacturing method of rapid catalytic dyeing paper, in particular to a low-cost and high-quality manufacturing method, and the manufacturing method of rapid catalytic dyeing paper can be applied in the field of colored dyed paper, such as wedding ribbon paper and colorful fireworks paper , Ordinary yellow paper and other fields. Background technique [0002] Dyeing paper has developed rapidly in China in recent years, and the domestic demand is relatively large, but the production cost of the product is too high, the color of the product is not bright enough, and the combination of dye and fiber is not sufficient, resulting in a large amount of waste of dye, hindering the health of the dyed paper industry develop. At present, the production of dyed paper mainly adopts the method of adding dyes to achieve the required bright color, but due to the existence of lignin, the color of the product will be dark. At the sam...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21H21/14D21H17/03D21H17/63
Inventor 刘德桃程凡陈进波路鹏博江宇豪
Owner SOUTH CHINA UNIV OF TECH
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