Method for refining rape-seed raw oil
A crude oil and rapeseed technology, applied in the direction of oil/fat refining, fat production, etc., can solve the problems of poor deacidification effect, and achieve good deacidification effect and good deodorization effect.
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Embodiment 1
[0016] Embodiment 1 of the present invention provides a kind of crude rapeseed oil refining method, comprises the following steps:
[0017] a. Pretreatment: filter the rapeseed crude oil to remove impurities;
[0018] b. Degumming: Add the rapeseed crude oil after removing impurities into the reaction kettle, and add a citric acid solution with a mass concentration of 40% at the same time, mix evenly, the addition of the citric acid solution is 0.1% of the oil weight, and then carry out Degumming reaction, the degumming temperature is 50°C, and the degumming time is 1.5h;
[0019] c. Deacidification: keep the ambient temperature at 80°C, add a phosphoric acid solution with a mass concentration of 1% to the degummed mixed solution, stir for 10 minutes, then add a sodium carbonate solution with a mass concentration of 3%, and mix and stir for 15 minutes. The addition of solution and sodium carbonate solution is 0.2% of the weight of the mixed solution, filter, and add hot water...
Embodiment 2
[0026] Embodiment 2 of the present invention provides a kind of crude rapeseed oil refining method, comprises the following steps:
[0027] a. Pretreatment: filter the rapeseed crude oil to remove impurities;
[0028] b. Degumming: Add the rapeseed crude oil after removing impurities into the reaction kettle, and add a citric acid solution with a mass concentration of 55% at the same time, mix evenly, the addition of the citric acid solution is 0.2% of the oil weight, and then carry out Degumming reaction, the degumming temperature is 60°C, and the degumming time is 2h;
[0029] c. Deacidification: Keep the ambient temperature at 100°C, add a phosphoric acid solution with a mass concentration of 2% to the degummed mixture, stir for 10 minutes, then add a sodium carbonate solution with a mass concentration of 4%, and mix and stir for 20 minutes. The addition of solution and sodium carbonate solution is 0.4% of the weight of the mixed solution, filter, and add hot water with a ...
Embodiment 3
[0035] Embodiment 3 of the present invention provides a kind of crude rapeseed oil refining method, comprises the following steps:
[0036] a. Pretreatment: filter the rapeseed crude oil to remove impurities;
[0037] b. Degumming: Add the rapeseed crude oil after removing impurities into the reaction kettle, and add a citric acid solution with a mass concentration of 43% at the same time, mix well, the addition of the citric acid solution is 0.15% of the oil weight, and then carry out Degumming reaction, the degumming temperature is 55°C, and the degumming time is 1.5h;
[0038] c. Deacidification: keep the ambient temperature at 90°C, add a phosphoric acid solution with a mass concentration of 1.5% to the degummed mixed solution, stir for 10 minutes, then add a sodium carbonate solution with a mass concentration of 3%, and mix and stir for 18 minutes. The addition of solution and sodium carbonate solution is 0.25% of the weight of the mixed solution, filter, add hot water w...
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