Preparation method of silver nano film for magnetic fluid deformable mirror
A technology of silver nanometer and deformable mirror, which is applied in the direction of optical components, optics, instruments, etc., can solve a large number of problems that cannot effectively control the thickness and uniformity of the film, and the surface is not glossy.
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[0010] This embodiment has the following processes and steps:
[0011] a. Take 12ml of 5mg / ml silver nanoparticle solution and put it in a centrifuge tube. After centrifuging at a speed of 3000r / s for 30min in the centrifuge, pour off the supernatant, leaving a light yellow substance at the bottom of the centrifuge tube, and then take ethanol As a solvent, the centrifugation operation was repeated 4 times to remove other impurities of the silver nanoparticle solution, and finally a pure silver nanoparticle ethanol solution was obtained;
[0012] b. the above-mentioned 12ml silver nanoparticles ethanol solution and 3ml 1mM active agent n-dodecanethiol ( ) were mixed, and the mixed solution was placed in an ultrasonic vibrator for 24 hours, and the incompletely reacted reagent was removed by repeated centrifugation to obtain pure silver nanoparticles wrapped in thiol, and then uniformly dispersed in ethyl acetate in the ester solution;
[0013] c. Use a micropipette to slowly...
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