Cold-etching agent displaying dendritic structure form of high-carbon steel continuous casting billet and preparation method
A technology of dendrite structure and continuous casting billet, which is applied in the field of cold etchant and its preparation, can solve problems such as corrosion inspection, and achieve the effect of simple operation, complete image and less pollution
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Embodiment 1
[0019] It is used to display the low-magnification dendritic structure of high-carbon steel continuous casting slabs containing C0.71%-0.82%, Mn0.5-0.8%, and Si0.15-0.35%.
[0020] Put 10 grams of ferric chloride, 1 gram of trinitrophenol, and 1.5 grams of cupric ammonium chloride into a glass container; take 1600 ml of distilled water, divide it into two parts, and add one part to the glass container , another backup. Stir the solid medicine until it is completely dissolved. Take 200 ml of absolute ethanol and add to spare distilled water. Take 25 ml of 32.3% hydrochloric acid and add it to the aqueous ethanol solution. After stopping for 2-5 minutes, pour the ethanol+hydrochloric acid aqueous solution into the aqueous solution containing ferric chloride, cupric ammonium chloride and trinitrophenol to form a comprehensive medicinal solution. Leave it for 8 hours to complete the preparation of the reagent.
[0021] Wipe the surface of the sample with a cotton pad dipped in...
Embodiment 2
[0023] It is used to display the low-magnification dendritic structure of high-carbon steel continuous casting slabs containing C0.82%-0.85%, Cr0.20%, and trace alloy elements V, Ti, and Nb.
[0024] Put 13 grams of ferric chloride, 2 grams of picric acid, and 2 grams of cupric ammonium chloride into a glass container. Take 2000 milliliters of distilled water and divide it into two parts. One part is added to the glass container, and the other is added to the glass container. A spare. Stir the solid medicine until it is completely dissolved. Add 300 ml of absolute ethanol to the spare distilled water. Take 30 ml of hydrochloric acid with a concentration of 32.3% and add it to the aqueous ethanol solution. After stopping for 2-5 minutes, pour the ethanol+hydrochloric acid aqueous solution into the aqueous solution containing ferric chloride, cupric ammonium chloride and trinitrophenol to form a comprehensive medicinal solution. Let it stand for 8 hours to complete the prepar...
Embodiment 3
[0027] It is used to display the low-magnification dendrite structure morphology of high-carbon steel continuous casting slabs containing 0.85% to 0.91% of C and containing trace amounts of V, Ti, Ni, and other alloying elements.
[0028] Put 15 grams of ferric chloride, 3 grams of picric acid, and 3 grams of cupric ammonium chloride into a glass container, take 2000 milliliters of distilled water, and divide it into two parts, one part is added to the glass container, and the other A spare. Stir the solid medicine until it is completely dissolved. Add 400 ml of absolute ethanol to the spare distilled water. Take 40 ml of 32.3% hydrochloric acid and add it to the aqueous ethanol solution. After stopping for 2-5 minutes, pour the ethanol+hydrochloric acid aqueous solution into the aqueous solution containing ferric chloride, cupric ammonium chloride and trinitrophenol to form a comprehensive medicinal solution. Leave it for 8 hours to complete the preparation of the reagent....
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