Yb-doped fiber and manufacturing method thereof
A technology of ytterbium-doped optical fiber and optical fiber, which is applied in the direction of cladding optical fiber, multi-layer core/clad optical fiber, light guide, etc., can solve the problems of central concave optical fiber refractive index and offset, and achieve the effect of high cladding absorption
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Embodiment 1
[0033] Embodiment 1: A pure quartz glass liner with a specification of 31mm (outer diameter of the tube)*1.8mm (thickness of the tube)*600mm (length of the tube) is fixed on an MCVD lathe, and a pure silicon outer cladding is deposited according to the design, and the deposition temperature is 1780°C , the flow rate of oxygen is 1000sccm, the flow rate of silicon tetrachloride is 400sccm, and the inner cladding layer is deposited after the outer cladding is deposited. , and then deposit the loose porous structure of the core layer, the deposition temperature is 1400°C, the flow rate of oxygen is 800 sccm, the flow rate of silicon tetrachloride is 200 sccm, and the flow rate of phosphorus oxychloride is 100 sccm. After the deposition is completed, the liner is removed, and the prepared Al and Yb solutions are poured Immerse in the liner for 4 hours, in which the concentration of aluminum chloride is 0.55mol / L, and the concentration of ytterbium chloride is 0.1mol / L. After the im...
Embodiment 2
[0034] Embodiment 2: A pure quartz glass liner with a specification of 31mm (outer diameter of the tube)*1.8mm (thickness of the tube)*600mm (length of the tube) is fixed on an MCVD lathe, and a pure silicon outer cladding is deposited according to the design, and the deposition temperature is 1780°C , the flow rate of oxygen is 1000sccm, the flow rate of silicon tetrachloride is 400sccm, and the inner cladding layer is deposited after the outer cladding is deposited. , and then deposit the loose porous structure of the core layer, the deposition temperature is 1400°C, the flow rate of oxygen is 800 sccm, the flow rate of silicon tetrachloride is 200 sccm, and the flow rate of phosphorus oxychloride is 70 sccm. After the deposition is completed, the liner is removed, and the prepared Al and Yb solutions are poured Immerse in the liner for 4 hours, in which the concentration of aluminum chloride is 0.65mol / L, and the concentration of ytterbium chloride is 0.12mol / L. After immers...
Embodiment 3
[0035] Embodiment 3: A pure quartz glass liner with a specification of 31mm (outer diameter of the tube)*1.8mm (thickness of the tube)*600mm (length of the tube) is fixed on an MCVD lathe, and a pure silicon outer cladding is deposited according to the design, and the deposition temperature is 1780°C , the flow rate of oxygen is 1000sccm, the flow rate of silicon tetrachloride is 400sccm, and the inner cladding layer is deposited after the outer cladding is deposited. , and then use the vapor phase method to deposit the vitrified core layer structure, the deposition temperature is 1900°C, the flow rate of oxygen is 800 sccm, the flow rate of silicon tetrachloride is 100 sccm, the flow rate of aluminum chloride is 100 sccm, the flow rate of ytterbium chloride is 100 sccm, the flow rate of phosphorus oxychloride is 50 sccm, and the flow rate of Freon 20sccm, after the core layer is deposited, it is melted and shrunk into a preform, and the shrinkage temperature is 2300°C. The co...
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