Water retention particle preparation method

A technology of water-retaining particles and ammonia water, applied in the field of super absorbent resin preparation, can solve the problems of no competitive advantage of products, increased production cost, time-consuming and labor-intensive, etc., and achieves the effects of unique measures, long water-retention time and simple process.

Active Publication Date: 2015-08-19
卢柳
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Other water-retaining agent production technologies require facilities and equipment such as jacketed pots with heating and cooling functions, and uniquely designed reactors; in addition, when these technologies produce water-retaining agent products, it takes several hours to polymerize and form water-retaining agents. time consuming and laborious
In addition, most of the water used in the production of existing water retaining agents is deionized water, and the production cost is relatively high
[0006] In addition, some water-retaining agent production technology still needs nitrogen gas in the production process, and requires polymerization in a specific environment. no competitive advantage

Method used

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Effect test

Embodiment Construction

[0025] Below in conjunction with embodiment the method of the present invention is further described.

[0026] A method for preparing water-retaining granules. In the technical proposal, the water-retaining granules are prepared by combining acrylic acid, acrylamide, ammonia water, ammonium persulfate, N.N-dimethylbisacrylamide, hydrosulfite and water.

[0027] The specific implementation is as follows:

[0028] The composition and proportioning of the raw materials are: 25 kg of acrylic acid, 25 kg of acrylamide, 25 kg of ammonia, 0.5 kg of ammonium persulfate, 0.3 kg of N.N-dimethylbisacrylamide, 0.25 kg of hydrosulfite, and 75 kg of water; In the reaction basin, dilute the above-mentioned acrylic acid with an appropriate amount of water, then add the above-mentioned acrylamide, and then stir evenly to obtain component A; in a beaker, use an appropriate amount of water to dissolve all the above-mentioned N.N-dimethylbisacrylamide in water Obtain component B; in a beaker, di...

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PUM

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Abstract

The invention relates to a water retention particle preparation method, wherein acrylic acid, acrylamide, ammonia water, ammonium persulfate, N.N-dimethyl bisacrylamide, sodium hyposulfite and water are combined and prepared into the water retention particles. According to the present invention, the whole production process does not require external auxiliary heating while the sodium hyposulfite is used as the self-initiation thermal agent, such that the temperature of the mixed liquid is automatically increased to achieve natural polymerization forming so as to form the product in a short time; the whole implementation process does not require relevant facilities and equipment while the simple facilities such as the corrosion resistance barrel, the disk and the like are utilized so as to substantially reduce the investment risk; the production process is not limited by the production environment, the full-opening type production can be achieved at the room temperature, even at the low temperature, and the efficient and high-quality water retention particles can be produced within 1 h; and the opening type reaction polymerization is performed during the implementation process, such that the reaction heat dispersion is easily achieved, the product cross-linking is uniform, the grafting rate is increased, and the performance is stable.

Description

technical field [0001] The invention belongs to the technical field of superabsorbent resin preparation, and in particular relates to a preparation method of water-retaining particles. Background technique [0002] Water absorbent resin (SuperAbsorbent Polymer, SAP) is a new type of functional polymer material. It can absorb water hundreds to thousands of times its own weight, non-toxic, harmless, and non-polluting; it has extremely strong water absorption capacity and high water retention capacity, and the high molecular weight polymer obtained through acrylic acid polymerization → high water retention capacity, absorbing under high load The absorbed water cannot be squeezed out by simple physical methods, and it can release and absorb water repeatedly. Applied in agriculture and forestry, it can form "micro reservoirs" in the roots of plants. In addition to absorbing water, super absorbent resin can also absorb fertilizers and pesticides, and release them slowly to incre...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F220/06C08F220/56C08F222/38
Inventor 卢柳
Owner 卢柳
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