Active carbon preparation method and device
A technology for preparing activated carbon and activated carbon, applied in the field of carbon materials, can solve the problems of high economic cost, non-renewability, unfavorable process sustainable development, etc., and achieve the effects of high environmental protection value, avoiding pollution, and huge economic benefits.
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[0078] The equipment for preparing activated carbon provided by the present invention includes a waste slag feeding device, and the waste slag feeding device is used to transport the waste slag described in the above technical solution to a material mixing device for mixing with the catalyst. In an embodiment of the present invention, in order to dry and pulverize the waste slag, the waste slag feeding device may include a waste slag storage device; a first drying device whose feeding port is connected to the discharge port of the waste slag storage device; A filter device in which the feed port is connected to the discharge port of the first drying device. In an embodiment of the present invention, the waste residue storage device is used to store furfural residue and / or xylose residue obtained from production; the outlet of the waste residue storage device is connected to the feed inlet of the first drying device, and The material transported from the waste residue storage d...
Embodiment 1
[0104] The raw material uses air-dried corncobs, and its water content is 15%. After the corncobs are dedusted by vibrating sieves, they are crushed into 1-1.5cm corncob particles by a hammer mill, and then transported by the elevator to the acid mixing truck for acid mixing. The acid concentration is 5%±2%. The solid-to-liquid ratio of the obtained suspension is 1:0.3, and it is sent into the hydrolysis kettle through a belt conveyor. The volume of the hydrolysis kettle is 10 cubic meters, and the double kettle is operated in series. After filling the hydrolysis kettle, the pressure is 0.50MPa±0.05 MPa water vapor, the hydrolysis temperature is 145°C, and the hydrolysis takes 4 hours. The furfural stock solution obtained by hydrolysis is introduced into the subsequent process, and the gross aldehyde is extracted, and the furfural is continuously refined to obtain commercial furfural. The furfural slag in the kettle is discharged into the slag yard for standby.
Embodiment 2
[0106] The raw material uses air-dried corncobs, and its water content is 10%. After the corncobs are dedusted by the vibrating screen, they are crushed into 1-1.5cm corncob particles by a hammer mill, and then transported by the elevator to the acid mixing truck for acid mixing. The acid concentration is 8% ± 2%, and the amount of acid used is kept The solid-to-liquid ratio of the obtained suspension is 1:0.5, and it is sent to the hydrolysis kettle through a belt conveyor. The volume of the hydrolysis kettle is 10 cubic meters, and the double kettle is operated in series. After filling the hydrolysis kettle, the pressure is 0.70MPa±0.05 MPa water vapor, the hydrolysis temperature is 180°C, and the hydrolysis takes 2 hours. The furfural stock solution obtained by hydrolysis is introduced into the subsequent process, and the gross aldehyde is extracted, and the furfural is continuously refined to obtain commercial furfural. The furfural slag in the kettle is discharged into t...
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