Composite low-temperature coolant and preparation method and applications thereof
A cold storage agent and low-temperature technology, applied in applications, chemical instruments and methods, food preservation, etc., can solve the problems of low latent heat of phase change, low thermal conductivity, and affecting cold storage capacity, and achieve low cost, simple preparation method, and cold storage effect Good results
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Embodiment 1
[0020] A preparation method of a composite low-temperature cold storage agent, the specific steps are as follows:
[0021] 1) Prepare 7.5g of ethylene glycol, 5.75g of ammonium chloride, 5.0g of sodium chloride, 4.75g of calcium chloride, 1g of guar gum, 0.3g of citric acid, 1.5g of sodium tetraborate, and 74.2g of water according to the mass percentage;
[0022] 2) Mix ethylene glycol, calcium chloride, and water to form an aqueous solution;
[0023] 3) Mix ammonium chloride, sodium chloride, guar gum, citric acid, and sodium tetraborate and grind them thoroughly to obtain a mixture;
[0024] 4) Add the mixture in step 3) to the aqueous solution in step 2), and stir at a high speed. Keep the temperature at about 50°C while stirring. After stirring evenly, let it stand for cooling to obtain the cooling agent. After testing, its phase transition temperature is -34.6°C, and its latent heat of phase transition is 315 kJ / kg.
Embodiment 2
[0026] A preparation method of a composite low-temperature cold storage agent, the specific steps are as follows:
[0027] 1) Prepare 7.5g of ethylene glycol, 4.8g of ammonium chloride, 4.6g of sodium chloride, 4.8g of calcium chloride, 1g of guar gum, 0.3g of citric acid, 1.25g of sodium tetraborate, and 75.75g of water according to the mass percentage;
[0028] 2) Mix ethylene glycol, calcium chloride, and water to form an aqueous solution;
[0029] 3) Mix ammonium chloride, sodium chloride, guar gum, citric acid, and sodium tetraborate and grind them thoroughly to obtain a mixture;
[0030] 4) Add the mixture in step 3) to the aqueous solution in step 2), and stir at a high speed. Keep the temperature at about 50°C while stirring. After stirring evenly, let it stand for cooling to obtain the cooling agent. After testing, its phase transition temperature is -35.3°C, and its latent heat of phase transition is 355 kJ / kg.
Embodiment 3
[0032] A preparation method of a composite low-temperature cold storage agent, the specific steps are as follows:
[0033] 1) Prepare 7.5g of ethylene glycol, 6.3g of ammonium chloride, 4.6g of sodium chloride, 4.8g of calcium chloride, 1g of guar gum, 0.3g of citric acid, 1.25g of sodium tetraborate, and 74.25g of water according to the mass percentage;
[0034] 2) Mix ethylene glycol, calcium chloride, and water to form an aqueous solution;
[0035] 3) Mix ammonium chloride, sodium chloride, guar gum, citric acid, and sodium tetraborate and grind them thoroughly to obtain a mixture;
[0036] 4) Add the mixture in step 3) to the aqueous solution in step 2), and stir at a high speed. Keep the temperature at 50°C while stirring. After stirring evenly, let it stand for cooling to obtain the cooling agent. After testing, its phase transition temperature is -36.1°C, and its latent heat of phase transition is 335 kJ / kg.
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