Metal halide pellet of ceramic metal halide lamp, preparation method for metal halide pellet and mercury-free ceramic metal halide lamp
A technology of ceramic metal halide lamps and metal halide pills, which is applied in the manufacture of discharge tubes/lamps, components of gas discharge lamps, cold cathode manufacture, etc. Low, reduce the pressure of metal halide lamps and other issues, to achieve excellent photoelectric color comprehensive parameters, good color rendering, and the effect of eliminating the harm of mercury pollution
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Embodiment 1
[0044] A metal halide pill of a ceramic metal halide lamp is made of a complex formed by a first metal halide and a second metal halide zinc iodide; the mass ratio of the first metal halide to the second metal halide is 1:1; the mass fractions of thulium iodide, samarium iodide and thallium iodide in the first metal halide are respectively 50%, 5% and 45% respectively.
[0045] The preparation method of described golden halide pill, comprises the following steps:
[0046](1) The above-mentioned first metal halide and the second metal halide are weighed in proportion and mixed uniformly to form a mixture, which is placed in a quartz container with a nozzle; the mixture is pre-vacuumized at 110°C for 60 minutes, vacuum The degree is 0.01Mpa;
[0047] (2) Under the condition of a vacuum degree of 0.01Mpa, slowly heat the mixture at a heating rate of 1°C / min until it melts, and then continue to stir for 20 minutes, and spray the molten mixture from the nozzle, and the molten bead...
Embodiment 2
[0051] A metal halide pill of a ceramic metal halide lamp is made of a complex formed by a first metal halide and a second metal halide zinc iodide; the mass ratio of the first metal halide to the second metal halide is 2:1; the mass fractions of thulium iodide, samarium iodide and thallium iodide in the first metal halide are 70%, 7%, and 23%, respectively.
[0052] The preparation method of described golden halide pill, comprises the following steps:
[0053] (1) The above-mentioned first metal halide and the second metal halide are weighed in proportion, mixed uniformly to form a mixture, and placed in a quartz container with a nozzle; the mixture is pre-vacuumized at 130°C for 50 minutes, vacuum The degree is 0.01Mpa;
[0054] (2) Under the condition of a vacuum degree of 0.01Mpa, slowly heat the mixture at a heating rate of 2°C / min until it melts, and then continue to stir for 30 minutes, and spray the molten mixture from the nozzle, and the molten beads are in high-puri...
Embodiment 3
[0058] A metal halide pill of a ceramic metal halide lamp is made of a complex formed by a first metal halide and a second metal halide zinc iodide; the mass ratio of the first metal halide to the second metal halide is 10:1; the mass fractions of thulium iodide, samarium iodide and thallium iodide in the first metal halide are respectively 80%, 10% and 10% respectively.
[0059] The preparation method of described golden halide pill, comprises the following steps:
[0060] (1) The above-mentioned first metal halide and the second metal halide are weighed in proportion, mixed uniformly to form a mixture, and placed in a quartz container with a nozzle; the mixture is pre-vacuumized at 150°C for 40 minutes, vacuum The degree is 0.01Mpa;
[0061] (2) Under the condition of a vacuum degree of 0.01Mpa, slowly heat the mixture at a heating rate of 3°C / min until it melts, and then continue to stir for 50 minutes, and spray the molten mixture from the nozzle, and the molten beads are...
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