A kind of extraction process of total triterpenes of fern
An extraction process and a technology for total triterpenes, which are applied in the field of extraction technology of total triterpenes of fern, can solve problems such as complicated steps, no process of removing impurities from starch and sugar, troubles in the purification of total triterpenes, etc., and achieve low production cost, Simple to use effects
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Embodiment 1
[0019] Embodiment 1 A kind of extraction process of the total triterpenoids of Bracken, comprising the following steps:
[0020] (1) 0.5 kg of junima root is crushed and passed through a 10-mesh sieve to obtain junima root powder.
[0021] (2) Extract the Juma root powder with ethanol solution with a mass concentration of 50% at a temperature of 60°C, extract 3 times, each time for 0.5 h, and combine to obtain an extract, which is filtered to obtain a filtrate, which is in The extract was obtained by concentrating under reduced pressure at a temperature of 50°C.
[0022] Wherein: the mass volume ratio of the fern root powder and the ethanol solution is 1g:10mL.
[0023] (3) Add water to the extract to settle twice, after stirring, let stand at room temperature for 1 h, then filter to obtain sediment.
[0024] (4) Add absolute ethanol twice its mass to the sediment to dissolve to obtain a solution, add 50% of its volume of activated carbon to decolorize and remove impurities ...
Embodiment 2
[0027] Embodiment 2 A kind of extraction process of the total triterpenoids of Bracken, comprising the following steps:
[0028] (1) After 1kg of junima root is crushed and passed through a 40-mesh sieve, junima root powder is obtained.
[0029] (2) Extract the Juma root powder with ethanol solution with a mass concentration of 60% at a temperature of 70°C, extract 4 times, each time for 1 hour, and combine to obtain an extract, which is filtered to obtain a filtrate, which is in The extract was obtained by concentrating under reduced pressure at a temperature of 70°C.
[0030] Wherein: the mass volume ratio of fern root powder and ethanol solution is 1g:20mL.
[0031] (3) Add water to the extract and settle for 3 times, after stirring, let stand at room temperature for 2 hours, then filter to obtain sediment.
[0032] (4) Add absolute ethanol 5 times its mass to the sediment for dissolution to obtain a solution, add 40% of its volume of activated carbon to decolorize and re...
Embodiment 3
[0035] Embodiment 3 A kind of extraction process of the total triterpenoids of Bracken, comprising the following steps:
[0036] (1) After 10kg of junima root is crushed and passed through a 60-mesh sieve, junima root powder is obtained.
[0037] (2) Extract the Juma root powder with ethanol solution with a mass concentration of 95% at a temperature of 80°C, extract three times, each time for 2.5 hours, and combine to obtain an extract, which is filtered to obtain a filtrate, which is in The extract was obtained by concentrating under reduced pressure at a temperature of 60°C.
[0038] Wherein: the mass volume ratio of the fern root powder and the ethanol solution is 1g:30mL.
[0039] (3) Add water to the extract to settle twice, after stirring, let stand at room temperature for 3 hours, then filter to obtain sediment.
[0040] (4) Add anhydrous ethanol 3 times its mass to the sediment to dissolve to obtain a solution, add 70% of its volume of activated carbon to decolorize ...
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