Cigarette monomer spice Mal-Ser as well as preparation method and application thereof
A technology of monomers and fragrances, which is applied in the field of flavors and fragrances and tobacco processing to achieve high yield, improve the roundness and comfort of smoke, and have obvious effects
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Embodiment 1
[0028] Example 2
[0029] A preparation method for tobacco monomer spice Mal-Ser, comprising the steps of:
Embodiment 2
[0031] Example 3
[0032] A preparation method for tobacco monomer spice Mal-Ser, comprising the steps of:
Embodiment 3
[0034] (1) Structural characterization of the target product
[0035] Through infrared spectroscopy (IR), high-resolution mass spectrometry (HR-MS), carbon nuclear magnetic resonance spectroscopy ( 13 C-NMR) carried out structural characterization of the target product Mal-Ser obtained in the examples, and the chemical structural formula of Mal-Ser is as follows:
[0036] .
[0037] ,IR
[0038] The synthesized product is analyzed by the Thermo Nicolet Avatar370 infrared spectrometer of American Nicolet company, the results are shown in figure 1 . As shown in the picture, 3501.65cm -1 and 3196.01cm -1 It is the absorption peak produced by the stretching vibration of the carboxyl group affected by the hydrogen bond, 1758.58cm -1 It is the characteristic absorption peak of carbonyl, which also shows the existence of carboxyl; 2990.55cm -1 and 2938.67cm -1 It is the C-H stretching vibration of the saturated hydrocarbon group on the isopropylidene group, 1209.62cm -1 ,...
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