Method for preparing coconut shell activated carbon with silver controlled-release sterilizing function through hydrothermal reaction
A technology of coconut shell activated carbon and hydrothermal reaction, applied in chemical instruments and methods, water/sewage treatment, adsorption water/sewage treatment, etc., can solve the problems of high cost of electrochemical deposition and reduction, impregnation and doping Long operating time, many harmful chemical reagents, etc., to achieve the effect of eliminating secondary pollution, fast adsorption rate, and high mechanical strength
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Embodiment 1
[0023] Take 5.0 g of coconut shell activated carbon from Tangshan Jianxin Factory, wash off the floating dust and impurities on the surface of the activated carbon by ultrasonic oscillation, and dry it at a constant temperature of 105 °C for 12 hours as a raw material. Put 5.0g of activated carbon and 2.0g / L silver nitrate solution in a reaction kettle for 6h at 120°C, then wash with distilled water until no silver ions flow out, then dry the above activated carbon in a vacuum oven at 70°C for 4h, under nitrogen protection , and calcined at 500°C for 2 h to prepare silver-loaded activated carbon (10 7 / mL sterilization time is 35min).
Embodiment 2
[0025] Take 5.0 g of coconut shell activated carbon from Tangshan Jianxin Factory, wash off the floating dust and impurities on the surface of the activated carbon by ultrasonic oscillation, and dry it at a constant temperature of 105 °C for 12 hours as a raw material. Put 5.0g of activated carbon and 8.0g / L silver nitrate solution in a reaction kettle for 4h at 150°C, then wash with distilled water until no silver ions flow out, then dry the above activated carbon in a vacuum oven at 70°C for 4h, under nitrogen protection , and calcined at 500°C for 2 h to prepare silver-loaded activated carbon (10 7 / mL sterilization time is 35min).
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