Production method of preparing tricalcium phosphate and byproduct special fertilizer for mangos
A technology of tricalcium phosphate and production method, applied in chemical instruments and methods, applications, phosphorus compounds, etc., can solve problems affecting the quality of tricalcium phosphate products, influence on the purity of tricalcium phosphate products, environmental pollution, etc., and achieve significant environmental protection value. and economic benefits, make up for the cost of impurity removal, and reduce production costs
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Embodiment 1
[0046] A kind of production method of preparing tricalcium phosphate by-product mango special fertilizer, comprises the following steps:
[0047] (1) Intermediate slurry preparation: use phosphoric acid and carbonamide to react in a stirred reactor at a temperature of 105°C, and control the molar ratio of phosphoric acid and carbonamide to 1.9:1, and stir at a stirring speed of 50r / min After reacting for 50min, the intermediate slurry was obtained;
[0048] (2) Synthesis of tricalcium phosphate slurry: add calcium hydroxide solution with 1.3 times the molar weight of carbonamide to the intermediate slurry, and control the reaction temperature to 80°C. When the reaction reaches 50min, detect the pH value, and wait for When the pH value is 8, the reaction is terminated, and it is transferred to a cooling crystallizer, and the temperature is lowered to 40°C, so that tricalcium phosphate crystals are precipitated, and the content of nitrogen, phosphorus, and calcium in the crystal...
Embodiment 2
[0055] A kind of production method of preparing tricalcium phosphate by-product mango special fertilizer, comprises the following steps:
[0056] (1) Preparation of intermediate slurry: react phosphoric acid and carbonamide in a stirred reactor at a temperature of 115°C, and control the molar ratio of phosphoric acid and carbonamide to 2.1:1, stirring at a stirring speed of 50r / min After reacting for 50min, the intermediate slurry was obtained;
[0057] (2) Synthesis of tricalcium phosphate slurry: add calcium hydroxide solution with 1.5 times the molar weight of carbonamide to the intermediate slurry, and control the reaction temperature to 80°C. When the reaction reaches 50min, detect the pH value, and wait for When the pH value is 9, the reaction is terminated, and it is transferred to a cooling crystallizer, and the temperature is lowered to 38°C, so that tricalcium phosphate crystals are precipitated, and the content of nitrogen, phosphorus, and calcium in the crystalliza...
Embodiment 3
[0064] A kind of production method of preparing tricalcium phosphate by-product mango special fertilizer, comprises the following steps:
[0065] (1) Intermediate slurry preparation: use phosphoric acid and carbonamide to react in a stirred reactor at a temperature of 110°C, and control the molar ratio of phosphoric acid and carbonamide to 2:1, and stir at a stirring speed of 50r / min After reacting for 50min, the intermediate slurry was obtained;
[0066] (2) Synthesis of tricalcium phosphate slurry: add calcium hydroxide solution with 1.4 times the molar weight of carbonamide to the intermediate slurry, and control the reaction temperature to 80°C. When the reaction reaches 50min, detect the pH value, and wait for When the pH value is 8.5, the reaction is terminated, and it is transferred to a cooling crystallizer, and the temperature is lowered to 35°C, so that tricalcium phosphate crystals are precipitated, and the content of nitrogen, phosphorus, and calcium in the crystal...
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