Process for production of hard coat film
A manufacturing method, a technology for hard coating films, applied in the directions of chemical instruments and methods, devices for applying liquid to surfaces, coatings, etc.
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Embodiment 1
[0279] (Production of cellulose ester film)
[0280] · Preparation of silica dispersion
[0281] AEROSIL R812 (manufactured by Japan Aerosil Co., Ltd.) 10 parts by mass
[0282] (The average diameter of primary particles is 7nm)
[0283] 90 parts by mass of ethanol
[0284] The above materials were stirred and mixed with a dissolver for 30 minutes, and then dispersed with a Manton Gaulin. While stirring, 88 parts by mass of methylene chloride was added to the silica dispersion, and stirred and mixed in a dissolver for 30 minutes to prepare a silica dispersion dilution. Filtration was performed with a fine particle dispersion diluent filter (Advantec Toyo Co., Ltd.: polypropylene wound filter TCW-PPS-1N).
[0285]
[0286] (cellulose ester resin)
[0287] Cellulose triacetate A (cellulose triacetate synthesized from cotton linters, acetyl substitution degree 2.88, Mn=140000) 90 parts by mass
[0288] (additive)
[0289] X-1 5 parts by mass
[0290] X-12 4 parts by mas...
Embodiment 2
[0350] Except having made content of the plasticizer A in the cellulose ester film of a hard coat into 1 weight%, it was the same as Example 1.
Embodiment 3
[0352] Except having made content of the plasticizer A in the cellulose ester film of a hard coat into 20 weight%, it was the same as Example 1.
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