Graphene conductive polyester fibers and preparation method thereof
A polyester fiber and graphene technology, applied in the manufacture of conductive/antistatic filaments, single-component polyester artificial filaments, melt spinning, etc., can solve problems such as dust absorption, electrostatic interference, and malignant accidents. Achieve the effect of simple production process, long-lasting conductivity and good dyeing performance
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Embodiment 1
[0020] 1) The purchased graphene has been functionalized with sulfonic acid groups on the surface, and the particle size of graphene is less than 1 micron, with good dispersion. Stir, mix, and disperse graphene, carbon nanotubes, and polyvinylpyrrolidone according to a mass ratio of 2:2:1 to obtain conductive particles; add conductive particles to polyester powder, and the amount of conductive particles added is polyester powder 5% of the mass percentage, the graphene superconducting masterbatch is prepared by a twin-screw granulation process.
[0021] 2) Two-component composite spinning technology to prepare graphene conductive polyester fiber
[0022] According to step 1), the graphene superconducting masterbatch obtained is dried and melted to obtain graphene superconducting polyester component a, and component a and ordinary polyester component b without conductive particles are spun into composite graphite by mixed spinning technology Acrylic conductive polyester fiber. ...
Embodiment 2
[0025] 1) The purchased graphene has been functionalized with sulfonic acid groups on the surface, and the particle size of graphene is less than 1 micron, with good dispersion. Stir, mix, and disperse graphene, carbon nanotubes, and polyvinylpyrrolidone according to a mass ratio of 2:1:1 to obtain conductive particles; add conductive particles to polyester powder, and the amount of conductive particles added is polyester powder The mass percentage is 10%, and the graphene superconducting masterbatch is prepared by a twin-screw granulation process.
[0026] 2) Graphene conductive polyester fiber prepared by single-component blend spinning technology
[0027] After the graphene superconducting masterbatch obtained according to step 1) is dried, it is melted and extruded by a screw extruder through the melt direct spinning online flexible addition technology, and metered by a metering pump into a dynamic mixer for stirring and mixing with the polyester melt. Then it is mixed ev...
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