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Multifunctional fabric fire retardant as well as preparation method and application of fabric fire retardant

A flame retardant, multi-functional technology, applied in textiles and papermaking, chemical instruments and methods, plant fibers, etc., can solve the problems of high cost, large waste discharge, long time consumption, etc., achieve excellent flame retardant effect, reduce finishing Cost, Emission Reduction Effect

Active Publication Date: 2014-08-13
约克夏染料(中山)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] On the other hand, most of the current domestic fabric treatment agents can only complete a certain function such as washing, softness, low bacteria, low yellowing, and flame retardancy. They have single functions, low efficiency, high cost, long time consumption, and large waste emissions. , serious environmental pollution and other issues, which are not in line with the country's proposal to build a resource-saving and environment-friendly society

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Multifunctional fabric fire retardant as well as preparation method and application of fabric fire retardant
  • Multifunctional fabric fire retardant as well as preparation method and application of fabric fire retardant
  • Multifunctional fabric fire retardant as well as preparation method and application of fabric fire retardant

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0038] (1) In a 2-liter four-necked round-bottomed flask equipped with a stirrer, a thermometer and a dropping funnel, add 1 liter of dichloromethane, 101 grams of triethylamine (1mol) and 101 grams of Slowly add 151.8 g of POCl at 5-10 °C 3 (1mol), after adding, stir at room temperature for 5 hours, and the resulting mixture directly proceeds to the next step without separation and characterization;

[0039] (2) In a 2-liter four-necked round-bottomed flask equipped with a stirrer, a thermometer and a dropping funnel, add 1 liter of methanol, 58 grams of OHCCHO (1mol) and 230 grams of (1mol), after fully stirring evenly, add 38 grams of sodium borohydride (1mol) in batches at a temperature of 5-10°C, react at room temperature for 5-10 hours, then add 1 liter of water to the reaction system, extract the organic phase, the organic phase Then wash twice with 1 liter of saturated brine, dry the organic phase with anhydrous sodium sulfate, filter to remove the desiccant, distil...

example 2

[0043] (1) In a 2-liter four-necked round-bottomed flask equipped with a stirrer, a thermometer and a dropping funnel, add 1 liter of dichloromethane, 101 grams of triethylamine (1mol) and 101 grams of Slowly add 151.8 g of POCl at 5-10 °C 3 (1mol), after adding, stir at room temperature for 5 hours, and the resulting mixture directly proceeds to the next step without separation and characterization;

[0044] (2) In a 2-liter four-neck round-bottomed flask equipped with a stirrer, a thermometer and a dropping funnel, add 1 liter of methanol, 72 grams of and 230 grams (1mol), after fully stirring evenly, add 38 grams of sodium borohydride (1mol) in batches at 5-10°C, react at room temperature for 5-10 hours, then add 1 liter of water to the reaction system, extract the organic phase, and then Wash twice with 1 liter of saturated brine, dry the organic phase with anhydrous sodium sulfate, filter out the desiccant, and distill the organic solvent under reduced pressure to di...

example 3

[0048] (1) In a 2-liter four-necked round-bottomed flask equipped with a stirrer, a thermometer and a dropping funnel, add 1 liter of dichloromethane, 101 grams of triethylamine (1mol) and 101 grams of Slowly add 151.8 g of POCl at 5-10 °C 3 (1mol), and then stirred at room temperature for 5 hours after the addition. The resulting mixture is directly carried out to the next step without separation and characterization;

[0049] (2) In a 2-liter four-necked round-bottomed flask equipped with a stirrer, a thermometer and a dropping funnel, add 1 liter of methanol, 58 grams of OHCCHO (1mol) and 244 grams of (1mol), after fully stirring evenly, add 38 grams of sodium borohydride (1mol) in batches at 5-10°C, react at room temperature for 5-10 hours, then add 1 liter of water to the reaction system, extract the organic phase, and then Wash twice with 1 liter of saturated brine, dry the organic phase with anhydrous sodium sulfate, filter out the desiccant, and distill the organic...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention discloses a multifunctional fabric fire retardant as well as a preparation method and application of the fabric fire retardant. The structural formula of the fire retardant is as shown in the specification, wherein in the structural formula, the n is great than or equal to 2 and less than or equal to 10; R<1> is one of H, C(1-6) saturated aliphatic hydrocarbon, C(2-6) unsaturated alkyl and a compound with the structural formula shown in the specification; in the compound, the m is great than or equal to 1 and less than or equal to 10; the R<2> is one of H and C(1-6) saturated aliphatic hydrocarbon; the R<3> is one of H and C(1-6) saturated aliphatic hydrocarbon; R<4> is one of H and C(1-6) saturated aliphatic hydrocarbon. The fire retardant disclosed by the invention belongs to an intumescent fire retardant containing two fire-retardant elements, namely nitrogen and phosphorus and is excellent in fire-retardant effect; N-O bonds and quaternary ammonium ions are contained in molecules and the fire retardant has the functions of low yellowing and sterilization, so that multistep finishing can be realized in one time, the finishing cost of fabrics is greatly reduced and the pollutant discharge amount of printing and dyeing industry can be greatly reduced.

Description

【Technical field】 [0001] The invention relates to a multifunctional fabric flame retardant and its preparation method and application, belonging to the technical field of textile chemical industry. 【Background technique】 [0002] Polymer materials have many superior properties and are widely used in textiles, electronics, machinery, chemicals, aerospace and other fields. With the improvement of people's awareness of fire prevention and the enhancement of the concept of disaster reduction and disaster prevention, people's requirements for flame retardant materials are getting higher and higher, which makes the development, production, promotion and application of flame retardants develop rapidly. Increasingly, the output has risen sharply. [0003] There are usually two ways to prepare flame-retardant textiles. One is the additive type, that is, the flame retardant is mixed with the spinning dope, so that the spun fabric has flame-retardant properties. The other is the post...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M13/453C07F9/6581D06M101/06
Inventor 张鑫宇尹标林张智慧李峥嵘宫国良
Owner 约克夏染料(中山)有限公司
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