Perfume composition for fenugreek tobacco and preparation method thereof
A technology for tobacco spice and fenugreek, applied in the field of fenugreek tobacco spice composition and preparation thereof, can solve the problems of restricted quality, great irritation, poor aftertaste, etc., and achieves improved aroma quality and aroma concentration, and reduced irritation. , to avoid the effect of mixing
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Embodiment 1
[0016] (1) Take the dried fenugreek and grind it, and then carry out microwave stirring extraction with water after crushing. The microwave extract was concentrated in vacuum until no water flowed out to prepare the microwave water extract of Fenugreek; (2) Another dried Fenugreek was crushed, and after crushing, it was stirred and extracted with 95wt% ethanol, and the ratio of solid to liquid was 1 : 4, the extraction time is 3 hours, the extraction temperature is 40°C, vacuum concentration is carried out after extraction, and the ethanol extract of fenugreek is prepared; (3) another dried fenugreek is mechanically ground, and the mesh number of fenugreek is 500 mesh , after grinding, the fenugreek is subjected to supercritical extraction, the extraction pressure is 25MPa, the extraction time is 3h, only the primary separation is performed, the primary separation pressure is 8.5MPa, and the primary separation is collected, which is the supercritical extract of fenugreek; (4) ...
Embodiment 2
[0018] (1) Take the dried fenugreek and grind it, and then carry out microwave stirring extraction with water after crushing. The microwave extract was concentrated in vacuum until no water flowed out to prepare the microwave water extract of Fenugreek; (2) Another dried Fenugreek was crushed, and after crushing, it was stirred and extracted with 95wt% ethanol, and the ratio of solid to liquid was 1 : 4, the extraction time is 3 hours, the extraction temperature is 40°C, vacuum concentration is carried out after extraction, and the ethanol extract of Fenugreek is prepared; (3) Another dried Fenugreek is mechanically ground, and ground until the mesh number of Fenugreek is 400 mesh , after grinding, the fenugreek is subjected to supercritical extraction, the extraction pressure is 25MPa, the extraction time is 3h, only the primary separation is performed, the primary separation pressure is 8.5MPa, and the primary separation is collected, which is the supercritical extract of fen...
Embodiment 3
[0020] (1) Take the dried fenugreek and grind it, and then carry out microwave stirring and extraction with water after grinding. The microwave extract was concentrated in vacuum until no water flowed out to prepare the microwave water extract of Fenugreek; (2) Another dried Fenugreek was crushed, and after crushing, it was stirred and extracted with 95wt% ethanol, and the ratio of solid to liquid was 1 : 4, the extraction time is 3 hours, the extraction temperature is 40°C, vacuum concentration is carried out after extraction, and the ethanol extract of Fenugreek is prepared; (3) Another dried Fenugreek is mechanically ground, and ground until the mesh number of Fenugreek is 450 mesh , after grinding, the fenugreek is subjected to supercritical extraction, the extraction pressure is 25MPa, the extraction time is 3h, only the primary separation is performed, the primary separation pressure is 8.5MPa, and the primary separation is collected, which is the supercritical extract of...
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