Rice wine vinasse extractive as well as preparation method and application thereof
A technology of extract and distiller's grains, which is applied in the field of rice wine distiller's grains extract and its preparation and application, can solve the problems of lack of effective utilization and low utilization value of rice wine distiller's grains, and achieve the effect of comprehensive utilization and increased economic value
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Embodiment 1
[0039] Example 1 Preparation of Rice Wine Distillers Grains Extract Dry Powder
[0040] Preparation steps include:
[0041] (1) Secondary fermentation of rice wine distiller's grains: add 900ml of distilled water to 300g of rice wine distiller's grains, stir and ferment at 40°C for 4 hours to obtain material liquid 1;
[0042] (2) Enzymolysis: Add 1g / L compound flavor protease of material solution 1 and β-glucanase of 1g / L material solution 1 to the material solution 1 obtained in step (1), and enzymolyze 4 at 55°C After 1 hour, the system was heated to 80°C for 30 minutes to inactivate the enzyme, and then filtered, and the filtrate was clarified after filtration, namely feed liquid 2;
[0043] (3) Purification and concentration: Add activated carbon accounting for 2% of the mass percentage of the feed liquid to the feed liquid 2, heat at 60°C for decolorization and deodorization for 60 minutes, filter the decolorized and deodorized feed liquid, and then use the filtrate wit...
Embodiment 2
[0045] Example 2 Preparation of Rice Wine Distillers Grains Extract Dry Powder
[0046] (1) Secondary fermentation of rice wine distiller's grains: add 900ml of distilled water to 300g of rice wine distiller's grains, stir and ferment at 40°C for 8 hours to obtain material liquid 1;
[0047] (2) Enzymolysis: Add 3g / L alkaline protease and 2g / L mannanase to the liquid 1 obtained in step (1), and enzymolyze it at 55°C for 4 hours , raise the temperature of the system to 80°C and keep it warm for 30 minutes to inactivate the enzyme, then filter, and the filtrate is clarified after filtration, that is, feed solution 2;
[0048] (3) Purification and concentration: Add activated carbon accounting for 1% of the mass percentage of the feed liquid to the feed liquid 2, heat at 60°C for decolorization and deodorization for 60 minutes, filter the decolorized and deodorized feed liquid, and then use the filtrate with a molecular weight cut-off of 2000 Dalton ultrafiltration membrane filt...
Embodiment 4
[0054] Example 4 Preparation of Rice Wine Distillers Grains Extract Dry Powder
[0055] Preparation steps include:
[0056] (1) Secondary fermentation of rice wine distiller's grains: add 300ml of distilled water to 300g of rice wine distiller's grains, stir and ferment at 50°C for 2 hours to obtain material liquid 1;
[0057] (2) Enzymolysis: Add 1g / L compound flavor protease of material solution 1 and β-glucanase of 5g / L material solution 1 to the material solution 1 obtained in step (1), and enzymolyze 16 After 1 hour, the system was heated to 80°C for 30 minutes to inactivate the enzyme, and then filtered, and the filtrate was clarified after filtration, namely feed liquid 2;
[0058] (3) Purification and concentration: Add activated carbon accounting for 5% of the mass percentage of the feed liquid to the feed liquid 2, heat at 60°C for decolorization and deodorization for 60 minutes, filter the decolorized and deodorized feed liquid, and then use the filtrate with a mol...
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