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Film-forming solution, and preparation method and application thereof

A film-forming liquid and glue liquid technology, which is applied in the direction of preserving meat/fish with a protective layer, protecting fruits/vegetables with a protective layer, coating, etc., can solve the problem of poor film-forming mechanical properties and needs to be further improved , easy to absorb moisture and sticky, etc., to achieve the effect of low cost, high production efficiency and good moisture resistance

Inactive Publication Date: 2014-03-26
UNIV OF SHANGHAI FOR SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The existing polysaccharide edible films and protein edible films mainly rely on intermolecular hydrogen bonds, intramolecular hydrogen bonds and special long-chain helical molecular structures to stabilize their chemical properties, but most of them are hydrophilic polymers , the moisture resistance is poor, which makes this type of film easy to absorb moisture and become sticky in a high humidity environment; although lipid edible films have good barrier properties, their film-forming properties and mechanical properties are often poor
The composite edible film can take into account the barrier properties, film-forming properties and mechanical properties of the film, but the formulation, production process and economical aspects of the composite edible film still need to be further improved

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] Table 1 is the formula of the film-forming liquid of Example 1, and each component in the formula is food grade. According to the formula in Table 1, calculate the mass of each component to obtain 500g of film-forming liquid.

[0022] The film-forming liquid formula of table 1 embodiment one

[0023] components

formula

quality score

Hordein

Hordein

5%

Nano-TiO 2 particle

Nano-TiO 2 particle

5%

gelling agent

sodium alginate

0.1%

Coagulant

calcium chloride

0.05%

plasticizer

Glycerin

3%

Antibacterial agents

Polylysine

2%

Aqueous ethanol

45% ethanol in water (v / v)

84.85%

[0024] Weigh 25g of hordein, add 300ml of 45% ethanol aqueous solution, and stir at 50°C for 2 hours to obtain glue A; dissolve 25g of nano titanium dioxide into 124.25ml of 45% ethanol aqueous solution, stir magnetically for 60min, then Ultrasonic oscillation was carried ...

Embodiment 2

[0028] Table 2 is the formula of the film-forming liquid of Example 2, and each component in the formula is food grade. According to the formula in Table 2, calculate the mass of each component to obtain 500g of film-forming liquid.

[0029] The film-forming liquid formula of table 2 embodiment two

[0030] components

formula

quality score

Hordein

Hordein

15%

Nano-TiO 2 particle

Nano-TiO 2 particle

1%

gel

carrageenan

0.1%

Coagulant

potassium citrate

3%

plasticizer

Glycerin

3%

Antibacterial agents

Polylysine

0.05%

Aqueous ethanol

55% ethanol in water (v / v)

77.85%

[0031] Weigh 75g of hordein, add 300ml of 55% ethanol aqueous solution, and stir magnetically at 50°C for 3 hours to obtain glue A; dissolve 5g of nano-titanium dioxide into 89.24ml of 55% ethanol aqueous solution, and magnetically stir for 40min. Then ultrasonically oscillate and dis...

Embodiment 3

[0035] Table 3 is the formulation of the film-forming solution in Example 3, and each component in the formulation is food grade. According to the formula in Table 3, calculate the mass of each component to obtain 500g of film-forming liquid.

[0036] The film-forming liquid formula of table 3 embodiment three

[0037] components

formula

quality score

Hordein

Hordein

10%

Nano-TiO 2 particle

Nano-TiO 2 particle

3%

gel

agar

2%

Coagulant

potassium chloride

1%

plasticizer

polyethylene glycol

2%

Antibacterial agents

Polylysine

0.15%

Aqueous ethanol

65% ethanol in water (v / v)

81.85%

[0038] Weigh 50g of hordein, add 350ml of 65% ethanol aqueous solution, and stir at 55°C for 2h to obtain glue A; dissolve 15g of nano-titanium dioxide into 59.25ml of 65% ethanol aqueous solution, stir magnetically for 50min, then Ultrasonic oscillation was carried out...

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Abstract

The invention provides a film-forming solution. The film-forming solution is characterized by comprising the following components: 5-30wt% of alcohol-soluble protein, 1-5wt% of nano TiO2 particles, 0.1-3wt% of gelatinizing agent, 0.05-3wt% of coagulant aid, 0.1-3wt% of plasticizer, and the balance of ethanol water of which the volume ratio is 45-65%. The invention also provides a method for preparing the film-forming solution. Furthermore, the invention also provides application of the film-forming solution as a food preservation film. According to the film-forming solution provided by the invention, not only are the edibility, the safety and the stability of the preservation film improved due to the alcohol-soluble protein, but also the preservation film is degradable and free of pollution to the environment. The nano TiO2 particles are contained, so that the film-forming solution has unique barrier property and mechanical property after a film is formed, and has an antibacterial effect. In addition, the preparation method of the film-forming solution provided by the invention is simple in process, and low in cost. The preservation film not only is good in moisture resistance, but also does not become tacky after being moistened, is degradable, green and environment-friendly, can well keep the quality of the food, and prolongs the shelf life after being formed on the food surface.

Description

technical field [0001] The invention belongs to the field of food packaging materials, and in particular relates to a film-forming liquid with gliadin as the main raw material, a preparation method of the film-forming liquid, and an application of the film-forming liquid as a coating type edible nano antibacterial fresh-keeping film. Background technique [0002] With the improvement of people's requirements for food quality and storage period and the enhancement of people's awareness of environmental protection, edible packaging films made of natural degradable materials have become a current research hotspot. Edible film is an edible film with certain packaging protection functions. It can be used as a barrier layer to maintain food quality and extend shelf life by controlling moisture migration, oxygen ingress, fat oxidation and loss of volatile substances. The existing edible films can be roughly divided into four categories according to raw materials: polysaccharide edi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D189/00C09D7/12A23B4/10A23B7/16
Inventor 管骁赵欣刘静
Owner UNIV OF SHANGHAI FOR SCI & TECH
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