Water-based gravure ink vehicle and preparation method thereof
A technology of gravure printing ink and connecting material, which is applied in the direction of ink, household appliances, application, etc., can solve the problems of harmful, polluting the environment, human body, limited chemical resistance and stability of raw materials, etc., and achieves simple process, fast drying speed, good gloss effect
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[0035] The preparation method of water-based gravure ink binder of the present invention specifically comprises the following steps:
[0036] Step 1, weigh 1%~8% epoxy resin E-44, 1%~8% ring opener, 2%~16% solvent, 5%~10% additives, 40%~80% Water-based polyurethane resin, 10% to 30% diluent, the total weight percentage of the above components is 100%, and the auxiliary agent is composed of catalyst, polymerization inhibitor, chain extender, crosslinking agent, defoamer and leveling agent mixture;
[0037] Use the solvent weighed in step 1 to dilute the epoxy resin, add the ring opener and mix evenly, and prepare under the condition of a constant temperature water bath at 60°C to 70°C:
[0038] Step 2, pour the epoxy resin E-44 diluted with ethyl acetate into the reaction container, add the polymerization inhibitor and catalyst evenly, stir evenly, and react in a constant temperature water bath at 60°C to 70°C for 4.5 hours while stirring at a low speed;
[0039] Step 3, addi...
Embodiment 1
[0042] Step 1, take the following components by weight percentage: 1% epoxy resin E-44, 2% solvent, 1% ring opener, 80% water-based polyurethane resin, 6% auxiliary agent, 10% diluent, wherein, auxiliary The agent is 1% catalyst, 0.5% polymerization inhibitor, 2.5% chain extender, 0.5% crosslinking agent, 0.5% leveling agent and 1% defoamer accounting for the total weight of the water-based gravure ink binder;
[0043] Among them, the ring-opening agent is diethanolamine; the solvent is ethyl acetate; the catalyst is triethanolamine; the polymerization inhibitor is hydroquinone; the chain extender is diethylene glycol (DEG); the crosslinking agent is SC- 100; the leveling agent is silicone acrylate; the defoamer is acetylene glycol DF-70 type; the diluent is deionized water;
[0044] Use the solvent weighed in step 1 to dilute the epoxy resin, add a ring opener and mix evenly, and prepare under the condition of a constant temperature water bath at 60°C-70°C:
[0045] Step 2, ...
Embodiment 2
[0050] Step 1, take the following components by weight percentage: 2% epoxy resin E-44, 4% solvent, 2% ring opener, 70% water-based polyurethane resin, 7% auxiliary agent, 15% diluent, wherein, auxiliary The agent is 1% catalyst, 0.5% polymerization inhibitor, 2.5% chain extender, 1% crosslinking agent, 0.5% leveling agent and 1.5% defoamer accounting for the total weight of water-based gravure ink binder;
[0051] Among them, the ring-opening agent is diethanolamine; the solvent is acetone; the catalyst is a mixture of N,N-dimethylethanolamine and N,N-dimethylformamide in a ratio of 1:1; the polymerization inhibitor is p-methoxy Phenol; chain extender is 4,4-dihydroxydiphenylpropane (BPA); crosslinking agent is polyether trihydric alcohol N330; leveling agent is silicone acrylate; defoamer is 504 surfactant; dilution The agent is a mixture of ethanol and deionized water in a ratio of 1:1;
[0052] Use the solvent weighed in step 1 to dilute the epoxy resin, add a ring opener...
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