Photochromic powder, photochromic glass and preparation method thereof
A photochromic glass and photochromic technology, applied in the direction of color-changing fluorescent materials, chemical instruments and methods, glass/slag layered products, etc., to achieve the effects of improved color-changing performance, less environmental pollution, and good color-changing performance
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[0027] Specifically, the photochromic film preparation method includes the following steps:
[0028] Provide polyvinyl butyral, plasticizer, coupling agent and the above-mentioned photochromic powder, the photochromic powder, polyvinyl butyral, plasticizer and coupling agent according to the following weight percentage mix to get a mixture;
[0029] Add the mixture to a mixer and stir for 10-20 minutes, heat it to 140-160°C to melt and extrude it into a film of 0.38-3.04mm, and then cool, remove water, blow dry, etc., to obtain photoinduced Color-changing film; the weight percentage of each component is as follows:
[0030]
[0031] Specifically, the polyvinyl butyral, plasticizer, coupling agent and photochromic powder are the same as those described above, and will not be repeated here.
[0032] The photochromic film of the embodiment of the present invention has a better color changing effect by selecting the above photochromic powder.
[0033] The embodiment of the p...
Embodiment 1
[0049] The preparation method of the photochromic glass of this embodiment comprises the following steps:
[0050] The first step is to prepare PVB photochromic film:
[0051] Get 85% by weight of polyvinyl butyral, 13.5% by weight of triethylene glycol di-n-heptanoate, 1.15% by weight of vinyltriethoxysilane and 0.35% by weight of helicopyran organic photochromic powder, uniform After mixing, add it to a mixer and stir for 10 minutes, heat to 150°C to melt and extrude to make a film, and after cooling, dewatering, drying, etc., a photochromic film is obtained;
[0052] The second step is to prepare photochromic laminated glass:
[0053] Clamp a piece of photochromic film prepared in Step 2 of the same area between two pieces of glass with clean surfaces, put them together in a silica gel bag, exhaust them under 2.5KPa vacuum for 20 minutes, and transfer them to a drying oven at 85°C Insulate for 30 minutes; then heat-press in an autoclave at 1.3MPa and 135°C for 25 minutes ...
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