Preparation method of poly[2, 5-dyhydroxy-1, 4-phenylene pyridine diimidazole] polymer
A technology of phenylenepyridine and dihydroxy, which is applied in the field of PIPD polymer preparation, can solve the problems of difficulty in stirring and conveying, low polymer molecular weight, etc., and achieve the effects of increasing molecular weight, reducing production cost, and facilitating stirring
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Embodiment 1
[0037] A kind of preparation method of poly[2,5-dihydroxyl-1,4-phenylene pyridodiimidazole] polymer, comprises the following processing steps:
[0038] A. Prepolymerization
[0039] Put 2,5-dihydroxyterephthalic acid (DHTA), tetraaminopyridine trihydrochloride monohydrate (TAP) and polyphosphoric acid (PPA) together into the polymerization kettle, mix well and remove hydrogen chloride gas, Carry out prepolymerization reaction then, obtain prepolymer;
[0040] B. After polycondensation
[0041] The discharge port of the polymerization kettle in step A is connected with the feed port of the twin-screw extruder, and the prepolymer is pressed into the described twin-screw extruder using dry nitrogen, and the prepolymer is extruded in the twin-screw extruder. After completing the post-condensation reaction in the machine, poly[2,5-dihydroxy-1,4-phenylenepyridinediimidazole] polymer was obtained; the reaction time of the prepolymer in the twin-screw extruder was 10min, The twin-s...
Embodiment 2
[0043] A kind of preparation method of poly[2,5-dihydroxyl-1,4-phenylene pyridodiimidazole] polymer, comprises the following processing steps:
[0044] A. Prepolymerization
[0045] Put 2,5-dihydroxyterephthalic acid (DHTA), tetraaminopyridine trihydrochloride monohydrate (TAP) and polyphosphoric acid (PPA) together into the polymerization kettle, mix well and remove hydrogen chloride gas, Carry out prepolymerization reaction then, obtain prepolymer;
[0046] B. After polycondensation
[0047] The discharge port of the polymerization kettle in step A is connected with the feed port of the twin-screw extruder, and the prepolymer is pressed into the described twin-screw extruder using dry nitrogen, and the prepolymer is extruded in the twin-screw extruder. After finishing the polycondensation reaction in the machine, a poly[2,5-dihydroxy-1,4-phenylenepyridinediimidazole] polymer was obtained; the reaction time of the prepolymer in the twin-screw extruder was 60min, The twin-s...
Embodiment 3
[0049] A kind of preparation method of poly[2,5-dihydroxyl-1,4-phenylene pyridodiimidazole] polymer, comprises the following processing steps:
[0050] A. Prepolymerization
[0051] Put 2,5-dihydroxyterephthalic acid (DHTA), tetraaminopyridine trihydrochloride monohydrate (TAP) and polyphosphoric acid (PPA) together into the polymerization kettle, mix well and remove hydrogen chloride gas, Carry out prepolymerization reaction then, obtain prepolymer;
[0052] B. After polycondensation
[0053] The discharge port of the polymerization kettle in step A is connected with the feed port of the twin-screw extruder, and the prepolymer is pressed into the described twin-screw extruder using dry nitrogen, and the prepolymer is extruded in the twin-screw extruder. After completing the post-condensation reaction in the machine, poly[2,5-dihydroxy-1,4-phenylenepyridinediimidazole] polymer was obtained; the reaction time of the prepolymer in the twin-screw extruder was 35min, The twin-s...
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