Activated carbon fiber ball and preparation method thereof
A technology of activated carbon fiber and small balls, which is applied in the direction of chemical instruments and methods, carbon compounds, and other chemical processes, can solve the problems of limiting the application range of activated carbon fiber, high cost of activated carbon fiber preparation, and difficult processing, etc., to achieve excellent oxidation resistance Excellent performance and corrosion resistance, improved activation efficiency, and high sphere strength
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Embodiment 1
[0021] A kind of active carbon fiber pellet, is made from the raw material of following parts by weight:
[0022] Activated carbon fiber 90, thermosetting resin carbon 2.5, phenolic emulsion 0.1, epoxy resin emulsion 5.
[0023] Its preparation method comprises the following steps:
[0024] (1) Stirring into balls: After mixing 0.1mm chopped carbon fiber and phenolic emulsion, use a high-speed mixer to stir into fiber pellets with a diameter of 2mm;
[0025] (2) Spheronization and granulation: Add epoxy resin emulsion to the carbon fiber pellets prepared in step (1) according to the solid content, and use a disc granulator to perform secondary spheronization to make fiber / resin with a diameter of 1.8mm small ball;
[0026] (3) Curing: Take the above fiber / resin pellets and cure them at 100°C for 2 hours to obtain cured pellets;
[0027] (4) Activation: place the solidified pellets in a carbonization activation furnace for carbonization, and activate them with water vapor at...
Embodiment 2
[0029] A kind of active carbon fiber pellet, is made from the raw material of following parts by weight:
[0030] Activated carbon fiber 97.5, thermosetting resin carbon 10, mixed solution 2 of polyvinyl alcohol aqueous solution and epoxy emulsion, mixed emulsion 20 of epoxy resin and phenolic resin.
[0031] Its preparation method comprises the following steps:
[0032] (1) Stirring into balls: After mixing 5mm chopped carbon fibers with a mixture of polyvinyl alcohol aqueous solution and epoxy emulsion, use a high-speed mixer to stir into fiber pellets with a diameter of 4mm;
[0033] (2) Spheronizing: Add the carbon fiber pellets prepared in step (1) to the mixed emulsion of epoxy resin and phenolic resin according to the solid content, and use a roller granulator to carry out secondary spheronizing to make a diameter of 3mm fiber / resin pellets;
[0034] (3) Curing: Take the above-mentioned fiber / resin pellets and cure them at 300°C for 10 hours to obtain cured pellets; ...
Embodiment 3
[0037] A kind of active carbon fiber pellet, is made from the raw material of following parts by weight:
[0038] Activated carbon fiber 93, thermosetting resin carbon 6, the liquid binder is a mixture of phenolic emulsion, polyvinyl alcohol aqueous solution, epoxy emulsion, and polyacrylamide aqueous solution 1, and the thermosetting resin emulsion is a mixture of epoxy resin, phenolic resin, and furfural resin emulsion Liquid 10.
[0039] Its preparation method comprises the following steps:
[0040] (1) Stirring into balls: After mixing 2mm chopped carbon fibers and liquid binders such as phenolic emulsion, polyvinyl alcohol aqueous solution, epoxy emulsion, and polyacrylamide aqueous solution, stir at high speed with a high-speed mixer to form a diameter of 3mm. fiber pellets;
[0041] (2) Spheronization and granulation: The carbon fiber pellets prepared in step (1) are added with a thermosetting resin emulsion according to the solid content to form a mixture of epoxy re...
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