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Preparation method of copper loaded activated carbon adsorbent

A technology of activated carbon and adsorbent, which is applied in the field of preparation of activated carbon adsorbent, can solve the problems of no method of finding adsorbent, no description of drying method and drying method, etc., and achieve the effect of avoiding uneven heating

Inactive Publication Date: 2014-01-15
冯良荣
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0011] Chinese patent CN1085114C discloses an adsorbent prepared by copper chloride, activated carbon, rare earth and attapulgite, but it does not explain the drying method and the effect of the drying method
[0013] In summary, in the existing sorbent literature, do not find the method for preparing sorbent similar to the present invention

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Carbon carrier: activated carbon, bulk density 0.38g / ml, BET specific surface area 1091m 2 / g, particle size 2.5mm, particle length 2-6mm.

[0025] Weigh CuCl 2 2H 2 O (analytical pure, molecular weight 170.48, content 99%) 60g was dissolved in 160ml distilled water to obtain solution A. Weigh 60 g of the above-mentioned activated carbon carrier into solution A, and immerse at 90° C. for 1 h. Filter then, pack activated carbon into the above-mentioned adsorption tower to form a high activated carbon packed column of about 50 cm, arrange two graphite electrodes at the two ends of the activated carbon column, one end of each graphite electrode is inserted in the activated carbon after impregnation, and the two graphite electrodes are additionally A voltage was applied at one end, and the impregnated activated carbon was heated to 200°C and dried for 20 minutes under a nitrogen atmosphere, and then cooled to room temperature under a nitrogen atmosphere. The surface of ...

Embodiment 2

[0028] Carbon carrier: activated carbon, bulk density 0.38g / ml, BET specific surface area 1091m 2 / g, particle size 2.5mm, particle length 2-6mm.

[0029] Weigh CuCl 2 2H 2 O (analytical pure, molecular weight 170.48, content 99%) 60g and glucose 30g were dissolved in 160ml distilled water to obtain solution B. Weigh 60 g of the above-mentioned activated carbon carrier into solution B, and immerse at room temperature for 3 h. Filter then, pack activated carbon into the above-mentioned adsorption tower to form a high activated carbon packed column of about 50 cm, arrange two graphite electrodes at the two ends of the activated carbon column, one end of each graphite electrode is inserted in the activated carbon after impregnation, and the two graphite electrodes are additionally A voltage was applied at one end, and the impregnated activated carbon was heated to 200° C. and dried for 90 minutes under a nitrogen atmosphere, and then cooled to room temperature under a nitrogen...

Embodiment 3

[0032] Carbon carrier: activated carbon, bulk density 0.38g / ml, BET specific surface area 1091m 2 / g, particle size 2.5mm, particle length 2-6mm.

[0033] Weigh Cu(NO 3 ) 2·3H 2 O (analytical pure, molecular weight 241.6, content 99%) 85g was dissolved in 160ml distilled water to obtain solution C. Weigh 60 g of the above-mentioned activated carbon carrier into solution C, and immerse at 90° C. for 3 h. Filter then, pack activated carbon into the above-mentioned adsorption tower to form a high activated carbon packed column of about 50 cm, arrange two graphite electrodes at the two ends of the activated carbon column, one end of each graphite electrode is inserted in the activated carbon after impregnation, and the two graphite electrodes are additionally A voltage is applied at one end, and the impregnated activated carbon is heated to 300° C. to dry and decompose for 20 minutes in an air atmosphere, and then cooled to room temperature in an air atmosphere. The surface o...

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Abstract

The invention provides a preparation method of an adsorbent for gas adsorbing separation. The adsorbent is used for the gas separation through pressure swing adsorption or temperature swing adsorption. The preparation method which treats activated carbon as a carrier comprises the following steps: dipping a copper salt and / or other assistants onto the active carbon carrier, placing the above obtained dipped activated carbon in a drying tower, and galvanizing the dipped activated carbon for heating the activated carbon in order to complete the drying process of the preparation of the adsorbent. The copper salt in the obtained adsorbent has a large load capacity and uniform dispersion on the surface of the activated carbon, so the adsorbent has a higher adsorption capability than traditional drying methods.

Description

technical field [0001] The invention provides a method for preparing a copper activated carbon adsorbent for gas adsorption and separation, which is used for pressure swing adsorption or temperature swing adsorption to separate gases. Background technique [0002] The pressure swing adsorption or temperature swing adsorption separation and purification process of gas is widely used because of its low energy consumption, operation at room temperature, high degree of automation, simple process, and devices that can be large or small. In 1985, Kawasaki Iron and Steel Corporation of Japan and Union Carbide Corporation of the United States built a 410Nm / h pressure swing adsorption purification CO device in Japan. The production capacity of a single set of large-scale CO PSA and hydrogen PSA separation and purification in the carbon-chemical industry and petrochemical industry has reached the scale of producing tens of thousands of cubic meters of gas per hour. [0003] At presen...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/20B01J20/30B01D53/04B01D53/047
Inventor 冯良荣甘亚张淑青
Owner 冯良荣
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