Preparation method of aqueous walnut leaf extract, walnut leaf alcohol solution obtained by using preparation method and application of walnut leaf alcohol solution
A technology of walnut leaves and water extracts is applied in the fields of preparation of water extracts of walnut leaves and extraction of active ingredients of walnut leaves, which can solve the problems of insufficient utilization and the like, and achieve the effects of inhibiting the regeneration of cancer cells, cleaning and high-efficiency preparation methods.
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Embodiment 1
[0028] The extraction steps of the present invention are as follows:
[0029] 1. Collect dead or fallen walnut leaves in Jinan or Tai'an area, clean them, dry them naturally until they are yellowish-brown, and store them in a dry place for later use;
[0030] 2. Weigh 2.5kg of walnut leaves and put them into the heating container (reactor), compact them so that the waste leaves are tightly placed in the heating container. After pressing the waste leaves, add water until the walnut leaves are covered by 10-20cm, generally about 15cm , soaked at room temperature for 2 hours;
[0031] 3. Install a condenser on the heating container, pass condensed water, pass nitrogen gas to the heating container, replace all the air in the container, and start heating the container in a nitrogen atmosphere until it boils, maintain the boiling state, and start Collect the distilled components; when the water level in the heating container drops to 2-4cm below the walnut leaves, add water to the ...
Embodiment 2
[0033] The extraction steps of the present invention are as follows:
[0034] 1. Collect dead or fallen walnut leaves in Jinan or Tai'an area, clean them, dry them until they are yellowish brown, and store them in a dry place for later use;
[0035] 2. Weigh 2.0kg of walnut leaves and put them into the heating container (reactor), compact them so that the waste leaves are tightly placed in the heating container. After pressing the waste leaves, add water until the walnut leaves are covered by 10-20cm, generally about 15cm , soak at 40°C for 1 hour;
[0036] 4. Install a condenser on the heating container, pass condensed water, pass nitrogen gas to the heating container, replace all the air in the container, and start heating the container in a nitrogen atmosphere until it boils, maintain the boiling state, and start Collect the distilled components; when the water level in the heating container drops to 2-4cm below the walnut leaves, add water to the heating container to the ...
Embodiment 3
[0038] The water extract of walnut leaves was extracted according to the method in Example 1, except that the walnut leaves were soaked at 70° C. for 30 min.
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