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Method for determining content of musk ketone in artificial musk

A technology of artificial musk and muscone, which is applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of complex measurement methods, achieve the effect of simple and reliable methods, and be conducive to industrialized mass production

Inactive Publication Date: 2013-06-19
上海永太医药科技有限公司
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  • Abstract
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  • Claims
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Problems solved by technology

However, the existing gas chromatography determination methods are relatively complicated

Method used

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  • Method for determining content of musk ketone in artificial musk
  • Method for determining content of musk ketone in artificial musk

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Embodiment Construction

[0021] The present invention is explained in detail below in conjunction with embodiment.

[0022] The method for muscone content in mensuration artificial musk of the present invention may further comprise the steps:

[0023] Step 1, making artificial musk need testing solution and muscone reference substance solution;

[0024] Step 2, adopt capillary gas chromatography, measure reference substance solution, make standard curve;

[0025] Step 3, measure muscone content in artificial musk need testing solution according to standard curve.

[0026] The invention adopts capillary gas chromatography, which is simple, fast and reliable, and is beneficial to industrialized production. The chromatographic column conditions of gas chromatography include:

[0027] Chromatographic column: fused silica (Rtx-5): 30 m×0.25 mm×0.25 μm;

[0028] Detector: hydrogen flame ionization detector (FID);

[0029] Temperature program: keep at 160 °C for 2.00 min, then raise the temperature to 2...

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Abstract

The invention provides a method for determining the content of musk ketone in artificial musk, and the method comprises the following steps: step 1, preparing the solution of an artificial musk test sample and musk ketone reference solutions; step 2, by using a capillary gas chromatography, assaying the reference solutions to acquire a standard curve; and step 3, determining the content of musk ketone in the artificial musk test sample according to the standard curve. The method for determining the content of musk ketone in artificial musk of the present invention is simple and reliable, thus being suitable for industrial mass production.

Description

technical field [0001] The invention relates to a method for determining the content of muskone, in particular to a method for determining the content of muskone in artificial musk by capillary gas chromatography. Background technique [0002] Musk is a rare and precious medicinal material commonly used in Chinese medicine clinics in my country. It has special functions such as resuscitating the mind, promoting blood circulation, and reducing swelling and pain. . Due to the shortage of musk deer resources, it is far from being able to meet the production and clinical application of many famous and expensive Chinese patent medicines. Therefore, the use of artificial musk instead of natural musk can supplement the shortage of musk deer resources. [0003] According to national regulations, the equivalent amount of artificial musk is used instead of musk. Because the quality standard of artificial musk has not been made public, the content of muscone, the main active ingredient...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/88
Inventor 朱子丰胡志刚王振玉王鸣杰王炳南
Owner 上海永太医药科技有限公司
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