Preparation method of ophoipogon japonicus extract and application thereof in cigarettes
A technology of Ophiopogon japonicus extract and Ophiopogon japonicus, which is applied in the extraction and application fields of natural plants, can solve the problems of inconsistent smoking sensation of cigarettes, excessive flakes and expanded cut tobacco, and deteriorated cigarette aroma quality, etc., so as to improve the quality of tobacco. Taste, ease of implementation, effect of improving tobacco aroma
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Embodiment 1
[0016] A preparation method of Ophiopogon japonicus extract and its application in cigarettes, the steps are as follows:
[0017] 1. Crush Ophiopogon japonicus medicinal material to 80 meshes, weigh 1Kg Ophiopogon japonicus Ophiopogon japonicus powder, heat and reflux extract once with 8 times the amount of 95% ethanol for 3 hours each time, filter, combine filtrates, and concentrate under reduced pressure to obtain a concentrated solution .
[0018] 2. Adsorb the concentrated solution on an AB-8 macroporous resin column (the ratio of medicinal material / resin is 1:2), first elute with water for 3 column volumes, and then use 40% ethanol for 3 column volumes, and collect 40% The ethanol eluted part is recovered, concentrated and dried to obtain the Ophiopogon japonicus extract.
[0019] 3. Take the Ophiopogon japonicus extract prepared above and dissolve it with 10 parts of water to prepare a dilution; take the dilution that accounts for 0.01% of the cut tobacco weight and add...
Embodiment 2
[0023] A preparation method of Ophiopogon japonicus extract and its application in cigarettes, the steps are as follows:
[0024] 1. Pulverize the Ophiopogon japonicus medicinal material to 80 meshes, weigh 1Kg Ophiopogon japonicus Ophiopogon japonicus powder, heat and reflux extraction with 15 times the amount of water for 3 times, each time for 1 hour, filter, combine the filtrates, and concentrate under reduced pressure to obtain a concentrated solution;
[0025] 2. Adsorption on HP-20 macroporous resin column on the concentrated solution (medicine material / resin ratio is 1:2), first eluted with water for 3 column volumes, then eluted with 20% ethanol for 3 column volumes, collected 20% The ethanol eluted part is recovered, concentrated and dried to obtain the Ophiopogon japonicus extract.
[0026] 3. Take the Ophiopogon japonicus extract prepared above and dissolve it with 10 parts of water to prepare a dilution; take the dilution which accounts for 0.03% of the cut tobacc...
Embodiment 3
[0030] A preparation method of Ophiopogon japonicus extract and its application in cigarettes, the steps are as follows:
[0031] 1. Grind the Ophiopogon japonicus medicinal material to 80 mesh, weigh 2Kg Ophiopogon japonicus Ophiopogon japonicus powder, heat and reflux extract with 10 times the amount of 30% ethanol twice, for 2 hours each time, filter, combine the filtrates, and concentrate under reduced pressure to obtain concentrated liquid;
[0032] 2. The concentrate is adsorbed on a HPD100 macroporous resin column (the ratio of medicinal material / resin is 1:5). First, 3 column volumes are eluted with water, and then 3 column volumes are eluted with 30% ethanol, and the 30% ethanol wash is collected. Partially removed, ethanol recovered, concentrated and dried to obtain the Ophiopogon japonicus extract.
[0033] 3. Take the Ophiopogon japonicus extract prepared above and dissolve it with 75% ethanol to prepare a dilution; take the dilution that accounts for 0.03% of the...
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