Method for preparing biological oil through catalytic liquefaction of microalgae
A bio-oil, microalgae technology, applied in the petroleum industry, producing fat, liquid carbon-containing fuel, etc., to achieve cost-saving effect
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Embodiment 1
[0032] The dried microalgae are pulverized in a pulverizer to obtain microalgae granules. Weigh 2.0 g of the treated microalgae, place it in a 17.2 mL batch autoclave, inject 6 MPa of hydrogen gas, and seal it. Put the autoclave into molten salt at 310°C, take out the autoclave after reacting for 20 minutes, and place it in water at room temperature for rapid cooling. After the reactor is cooled to room temperature, dry the reactor with a hair dryer, and then open the valve to depressurize the reactor. The reaction kettle was opened, the mixture in the kettle was poured out, the reaction mixture was extracted with dichloromethane, and the filter residue was removed by filtration to obtain an organic phase. The organic phase was removed by rotary evaporation with a rotary evaporator, and the remaining substance was bio-oil with a yield of 45.2wt.%.
Embodiment 2
[0034] The dried microalgae are pulverized in a pulverizer to obtain microalgae granules. Weigh 2.0 g of the treated microalgae, place it in a 17.2 mL batch autoclave, add 0.2 g of Pt / C catalyst, inject 6 MPa of hydrogen gas, and seal it. Put the autoclave into molten salt at 310°C, take out the autoclave after reacting for 20 minutes, and place it in water at room temperature for rapid cooling. After the reactor is cooled to room temperature, dry the reactor with a hair dryer, and then open the valve to depressurize the reactor. The reaction kettle was opened, the mixture in the kettle was poured out, the reaction mixture was extracted with dichloromethane, and the filter residue was removed by filtration to obtain an organic phase. The organic phase was removed by rotary evaporation with a rotary evaporator, and the remaining substance was bio-oil with a yield of 46.17wt.%.
Embodiment 3
[0036] The dried microalgae are pulverized in a pulverizer to obtain microalgae granules. Weigh 2.0 g of the treated microalgae, place it in a 17.2 mL batch autoclave, add 0.2 g of Pd / C catalyst, inject 6 MPa of hydrogen gas, and seal it. Put the autoclave into molten salt at 310°C, take out the autoclave after reacting for 20 minutes, and place it in water at room temperature for rapid cooling. After the reactor is cooled to room temperature, dry the reactor with a hair dryer, and then open the valve to depressurize the reactor. The reaction kettle was opened, the mixture in the kettle was poured out, the reaction mixture was extracted with dichloromethane, and the filter residue was removed by filtration to obtain an organic phase. The organic phase was removed by rotary evaporation with a rotary evaporator, and the remaining substance was bio-oil with a yield of 45.55wt.%.
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