Method for anhydride modified melamine resin
A technology for modifying melamine resin and acid anhydride, which is applied in the field of producing foam materials, and can solve problems such as the inability to obtain foam
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example 1
[0004] Example 1: Put 3000g of melamine and 3000g of maleic anhydride into a 10-liter high-mixer, feed circulating nitrogen, start stirring, stop heating when the temperature rises to 90 degrees Celsius, and continue stirring when the temperature rises to 150 degrees Celsius. Mix, 20 degrees centigrade cold water cools down side, and whole process 50 minutes, obtain light yellow powder 5870g. Put 10Kg of 36% industrial formaldehyde into the reactor, adjust the pH to 9 with 30% sodium hydroxide solution, start stirring, put the obtained 5870g light yellow powder into the reactor and start heating to 85 degrees Celsius, stop heating and cool down to 72 degrees Celsius and keep warm 8 hours. A colorless and transparent anhydride-modified melamine resin was obtained.
[0005] Take 200g of the above-mentioned anhydride-modified melamine resin, add K12 emulsifier 1.5g formic acid curing agent 4g pentane foaming agent 1g and stir quickly, put it into a microwave oven with a power of...
example 2
[0006] Example 2: Put 3,000g of melamine into a 10-liter high-mixer, feed in circulating nitrogen, start stirring, slowly add 3,000g of acetic anhydride, then start heating, stop heating when the temperature rises to 90 degrees Celsius, continue stirring, and put in Low mixing, 20 degrees Celsius cooling water release, the whole process is 55 minutes, to obtain 5900g of white powder. Put 20Kg of 36% industrial formaldehyde into the reactor, adjust the pH to 9 with 30% sodium hydroxide solution, start stirring, put 5900g of white powder and 6000g of melamine into the reactor at the same time, start heating to 85 degrees Celsius, stop heating and cool down to 72 Incubate for 8 hours after deg C. A colorless and transparent anhydride-modified melamine resin was obtained.
[0007] Take 200g of the above-mentioned anhydride-modified melamine resin, add OP-10 emulsifier 3g formic acid curing agent 4g pentane foaming agent 5g and stir rapidly, put it into a microwave oven with a pow...
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