Composite adsorption material for removing arsenic ions from natural water and preparation method for adsorption material
A composite adsorption material and adsorption material technology, applied in the field of waste water treatment in environmental protection, can solve the problems of complex process and high preparation cost of arsenic ion removal method, and achieve the effect of low cost, simple operation and wide source
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Embodiment 1
[0021] Weigh 20g of spent wheat grains through high-temperature pretreatment and add 100mL of Ca(OH) with a mass fraction of 8%. 2 Put the solution in a 250mL narrow-mouth glass bottle, shake it to make it gel for 13h, take it out and age it for 1d, wash it with deionized water, then wash it with absolute ethanol, filter it with suction, and put it in a muffle furnace at 300°C Burn in medium for 2 hours, take it out and cool it, and save it for later use; take an appropriate amount of modified spent wheat grains in a beaker, add distilled water and use a stirrer to fully stir the solution to adjust the solution to pH = 11, then prepare a suspension of 4.5g / L, and suspend it Slowly pour the solution into the 0.001mol / L hydroxy iron ion solution, stir well with a stirrer, stand and stand for 2 months, then centrifuge, discard the supernatant, rinse the obtained sediment several times with distilled water, and Dry and grind at a temperature of 50°C to obtain the adsorption materi...
Embodiment 2
[0024] Weigh 20g of spent wheat grains through high-temperature pretreatment and add 100mL of Ca(OH) with a mass fraction of 8%. 2 Put the solution in a 250mL narrow-mouth glass bottle, shake it to make it gel for 14 hours, take it out and age it for 2 days, wash it with deionized water, then wash it with absolute ethanol, filter it with suction, and put it in a muffle furnace at 300 °C Burn in medium for 3 hours, take it out and cool it, and save it for later use; take an appropriate amount of modified spent wheat grains in a beaker, add distilled water and use a stirrer to fully stir the solution to adjust the solution to pH = 11, then prepare a suspension of 4.5g / L, and suspend it Slowly pour 0.001 mol / L of hydroxy iron ion into the solution, stir well with a stirrer, stand and stand for 3 months, then centrifuge, discard the supernatant and rinse the obtained sediment several times with distilled water, Then dry and grind at a temperature of 55°C to obtain the adsorption m...
Embodiment 3
[0027] Weigh 20g of spent wheat grains through high-temperature pretreatment and add 100mL of Ca(OH) with a mass fraction of 8%. 2 Put the solution in a 250mL narrow-mouth glass bottle, shake it to make it gel for 16 hours, take it out and age it for 3 days, wash it with deionized water, then wash it with absolute ethanol, filter it with suction, and put it in a muffle furnace at 300 °C Burn in medium for 4 hours, take it out and cool it, and save it for later use; take an appropriate amount of modified spent wheat grains in a beaker, add distilled water and use a stirrer to fully stir the solution to adjust the solution to pH = 11, then prepare a suspension of 4.5g / L, and suspend it The solution was slowly poured into 0.001mol / L hydroxy iron ion solution, fully stirred evenly with a stirrer, left to stand for 4 months and then centrifuged, the supernatant was discarded, and the obtained sediment was rinsed with distilled water several times, and placed in Dry and grind at 60°...
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