A kind of manufacturing method of reconstituted tobacco leaf by papermaking method
A technology for reconstituting tobacco leaves and a manufacturing method, which is applied in the fields of tobacco, tobacco preparation, and application, can solve the problems of low product use ratio, large waste water treatment pressure, loss, etc., and achieve sensory comfort improvement, reduction of treatment pressure, and reduction of COD value. Effect
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Embodiment 1
[0021] Put 5 kg of flue-cured tobacco powder raw materials with a moisture content of 60 mesh or more and a moisture content of 5% into a 24L extraction kettle, extract for 2 hours at 50°C under an extraction pressure of 300mPa, use 70% ethanol as an entrainer, and use 10 times the water and washed 3 times to get the essential oil.
[0022] After supercritical extraction, the tobacco powder raw material and tobacco stem are mixed according to the weight ratio of 5:5, and 80 kg of water is added, extracted at 60°C for 1 hour, and then the extract is separated from the solid residue by pressing, filtering, and centrifuging. The purified extract is vacuum-concentrated at a vacuum of 80mPa and a temperature of 60°C until the weight content of solids in the concentrate reaches 50%, and the essential oil obtained after washing with water is added to the concentrate to make a dip coating Liquid, essential oils account for 0.3% of the entire dipping solution by weight. After the soli...
Embodiment 2
[0025] Add 5 kg of minced Burley tobacco with a moisture content of 25% above 60 mesh into a 24L extraction kettle, and extract for 2 hours at 50°C under an extraction pressure of 350mPa. The extract in the separation tank is rectified under the rectification conditions of 150°C tower bottom temperature, 100°C tower top temperature, and a reflux ratio of 5. The supercritical fluid tobacco extract is rectified, and the essential oil of the tower overhead distillate is used for dipping liquid preparation. ;
[0026] After supercritical extraction, burley tobacco powder and tobacco stems are mixed according to the weight ratio of 5:5, and 80 kg of water are added, extracted at 60°C for 1 hour, and then the extract and solid residue are separated by pressing, filtering, and centrifugation. separate. The purified extract is vacuum-concentrated at a vacuum of 80mPa and a temperature of 60°C until the weight content of solids in the concentrate reaches 50%, and the essential oil obt...
Embodiment 3
[0029] Add 5 kg of flue-cured tobacco powder with a moisture content of 60 mesh or more and a moisture content of 12% into a 24L extraction kettle, use 80% ethanol aqueous solution as an entrainer, and extract at 50°C under an extraction pressure of 350mPa for 2 hours. The extract in the separation kettle was molecularly distilled at different temperature ranges under the conditions of rotor speed 300 r / min and material flow rate 70 mL / h, and the product essential oil in the temperature range of 40-60 °C was collected for dipping liquid preparation.
[0030] After supercritical extraction, flue-cured tobacco powder and tobacco stems are mixed according to the weight ratio of 5:5, and 80 kg of water is added, extracted at 60°C for 1 hour, and then the extract is separated from the solid residue by pressing, filtering, and centrifuging. The purified extract is concentrated in vacuum until the weight content of solids in the concentrate reaches 50% under the conditions of a vacuum...
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