Method for preparing chitin nano filaments
A nanofibril, chitin technology, applied in the chemical characteristics of fibers, textiles and papermaking, etc., can solve the problems of short chitin nanofibrils, unable to meet market demands, etc. The effect of a uniform degree of fibrillation
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specific Embodiment approach 1
[0036] Specific embodiment one: the preparation method of a kind of chitin nanofibril provided in this embodiment, specifically is finished according to the following steps:
[0037] 1. Drying and pulverizing the biological raw material to obtain biological raw material powder; or directly pulverizing to obtain biological raw material powder, wherein the biological raw material is the exoskeleton of a crustacean containing chitin;
[0038] 2. Add lye to the biological raw material powder obtained in step 1 for processing, and obtain the biological raw material powder with partial protein removal;
[0039] 3. Add hydrochloric acid solution to the biological raw material powder obtained in step 2 to obtain demineralized salt and partial protein biological raw material powder;
[0040] Four, add lye to the biological raw material powder of demineralized salt and part protein obtained in step 3 and carry out further processing, obtain the biological raw material powder of deminera...
specific Embodiment approach 2
[0053] Embodiment 2: The difference between this embodiment and Embodiment 1 is that the biological raw material described in step 1 is shrimp shell or crab shell, and the particle size of the biological raw material powder is 50 mesh to 70 mesh. Others are the same as in the first embodiment.
specific Embodiment approach 3
[0054] Embodiment 3: The difference between this embodiment and Embodiment 1 or 2 is that the drying described in step 1 is drying at 50° C. to 105° C. for 10 minutes to 180 minutes. Others are the same as in the first or second embodiment.
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