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Reactor and a method of purifying a process solution

A reactor and solution technology, applied in the direction of chemical instruments and methods, improvement of process efficiency, chemical/physical/physical chemical fixed reactors, etc., can solve the problem of not easy to consider capacity flexibility, affecting the number of solution purification cycle stages, Problems such as increase in the amount of solid matter

Inactive Publication Date: 2012-11-14
OUTOTEC OYJ
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, as the reaction proceeds, the particle size of the solid material in the bed decreases, whereby the amount of solid material drifting with the solution increases
[0006] The disadvantage faced by current reactors is that in each reactor the flow passes through the fluidized bed once
This significantly affects the purification of the solution and the number of circulation stages
Furthermore, current fluidized bed reactors are not regulated, but their properties are determined according to the supply and particle size of the process stream
Naturally, this causes problems when these quantities vary according to the state of the process
In addition, the reactor is batch type, and it is not easy to consider the flexibility caused by capacity

Method used

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  • Reactor and a method of purifying a process solution
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  • Reactor and a method of purifying a process solution

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Embodiment Construction

[0021] Figure 1a Shows a reactor 1 according to the invention in which a liquid process solution 2 and solid matter are treated such that the powdered solid matter forms a fluidized bed 3 with the liquid and simultaneously with the process to be purified which is fed into the reactor Solution 2 reacts. In the fluidized bed 3, the flow fluidizes the solid matter reacting with the solution. According to this example, the displacement reaction in question is the removal of cadmium from a solution bearing zinc, wherein the aqueous solution, ie the solution bearing cadmium of the substance to be displaced, flows through a bed of zinc powder. Now, a reaction proceeds according to which zinc dissolves in the solution and cadmium is removed from the solution. In the lower part of the reactor, ie the cylindrical reaction part 4, a fluidized bed 3 is formed. From this lower part rises a conical upwardly widening calming part 5 and another cylindrical clarifying part 6 in order to lif...

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Abstract

The invention relates to a method and a reactor for purifying solid matter from the process solution (2) in the fluidized bed in the reactor, into which the process solution is fed to form the fluidized bed (4) in the essentially cylindrical reaction part (3) that is the lowermost part in the reactor, from which bed the flow further moves to the calming part (5) that expands conically upwards from the upper part of the reactor part and, further, to the cylindrical clarification part (6) that is connected to the upper part of the same, the diameter of the clarification part being the same as the upper part of the calming part, whereby at least part of the solution (2) that is fed into the reactor (1) is circulated to the fluidized bed (3) more than once, and that the amount of circulating solution is controlled in the fluidized bed by means of the mixing member (12) placed in the reactor.

Description

technical field [0001] The present invention relates to a device and a method as defined in independent claims 1 and 11 for purifying process solutions. Background technique [0002] Typically, stirred reactors are cylindrical and they have standard diameters. Typically, they are provided with flow resistances, which are attached to the walls of the reactor and whose purpose is to eliminate central turbulence, which is considered harmful and absorbs gas from the surface. Solid-solution processes generally require mixing in which strong turbulence and extensive circulation occur. An important process is the removal of cadmium, eg by displacement. Cadmium is one of the harmful substances in the electrolysis process of zinc. [0003] The feeding into the stirred reactor takes place primarily by feeding solid matter and solutions into the reaction space from above. Generally, in a continuous reactor, it is desirable for solid matter and solution to escape at approximately th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/20B01J19/18C22B3/02C22B3/20C22B3/46C22B17/00C22B19/00C22B19/20B01F7/22B01F27/91
CPCB01F7/22B01J8/20C22B3/20C22B19/26B01F7/168Y02P10/20B01F27/861B01F27/91B01J8/382C22B17/00C22B3/02C22B3/46B01F23/50
Inventor J·瓦尔诺M·劳娜拉
Owner OUTOTEC OYJ
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